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BSKANALYTICAL LABORATORIES QC Summary Report 12/30/2002 IIIIIIIIIIIIIIIIIIIIIII[llllllllllllllllllllillllllilllliil BSK Submission 2002120386 Client Caltest Analytical Laboratory Date Submitted 12106/2002 Project ID C120220 Project Desc BSK StarLltns Run# 47572 Instrument ID HPLC2 Analyst Initials TIMC Method Number 5491 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike LD Result Units or RPD RPD Cone Cone UCL LCL Date Diquat LDUP 272606 0 lig/L N/A ND 50 NIA 12/10/02 Acceptable Diquat MS 272589 372 pg/L 93 40 ND 150 50 12/10/02 Acceptable -------------------- -- ------------ Diquat ----------------------------------------------- T RBLK N/A 0 µg/1- <4 4 NIA 12/10/02 Acceptable BSK StarLlms Run# 47620 [I[I[IIIIIIIIII111II[1IIIIIIIIIlI Instrument ID GC7 Analyst Initials RACHELM Method Number 5153 Analyte Results Matrix %Ree Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Cone Cone UCL LCL Date 2,4,5-T LCS N/A 294 lig/L 96 304 ND 130 70 12/12/02 Acceptable 2,4,5-TP(Silvex) LCS N/A 3 19 µg/L 106 30 ND 130 70 12/12/02 Acceptable • 2,4-D LCS. N/A 2987 lig/L 95 313 ND 130 70 12/12/02 Acceptable Bentazon(Basagran) LCS N/A 578 I&L 95 606 ND 130 70 12/12/02 Acceptable Dalapon LCS N/A 2732 µg/L 90 30 1 ND 130 70 12/12/02 Acceptable Dicamba(Banvel) LCS N/A 463 µg/L 103 446 ND 130 70 12/12/02 Acceptable Dmoseb(DNBP) LCS N/A 607 gg/L 101 598 ND 130 70 12/12/02 Acceptable Pentachlorophenol(PCP) LCS N/A 059 Ag/L 96 060 ND 130 70 12/12/02 Acceptable Picloram LCS N/A 282 µg/L 95 294 ND 130 70 12/12/02 Acceptable 2,4,5-T LCSD NIA 29 pg/L 95 13 304 ND 130 70 12/12/02 Acceptable 2,4,5-TP(Silvex) LCSD N/A 3 06 µg/L 102 41 3 0 ND 130 70 12/12/02 Acceptable 2,4-D LCSD NIA 3002 µg/L 95 051 313 ND 130 70 12/12/02 Acceptable Bentazon(Basagran) LCSD N/A 571 µg/L 94 12 606 ND 130 70 12/12/02 Acceptable Dalapon LCSD N/A 2728 lig/L 90 014 30 1 ND 130 70 12/12/02 Acceptable Dicamba(Banvel) LCSD N/A 462 ;Ag/L 103 021 446 ND 130 70 12/12/02 Acceptable Dinoseb(DNBP) LCSD NIA 637 µg/1- 106 49 5 98 ND 130 70 12/12/02 Acceptable Pentachlorophenol(PCP) LCSD N/A 056 µg/1- 93 36 06 ND 130 70 12/12/02 Acceptable Picloram LCSD N/A 281 n/L 95 035 294 ND 130 70 12/12/02 Acceptable 2,4,5-T LDUP 272108 0 µg/L N/A ND 30 N/A 12/12/02 Acceptable 2,4,5-TP(Silvex) LDUP 272108 0 11811- N/A ND 30 N/A 12/12/02 Acceptable 2,4-D LDUP 272108 0 lig/L N/A ND 30 N/A 12/12/02 Acceptable Bentazon(Basagran) LDUP 272108 0 }ig/L N/A ND 30 N/A 12/12/02 Acceptable Dalapon LDUP 272108 0 lig/L N/A ND 30 N/A 12/12/02 Acceptable Dicamba(Banvel) LDUP 272108 0 lig/L N/A ND 30 NIA 12/12/02 Acceptable Dmoseb(DNBP) LDUP 272108 0 Ag/L N/A ND 30 N/A 12/12/02 Acceptable Pentachlorophenol(PCP) LDUP 272108 0 pg/L N/A ND 30 N/A 12/12/02 Acceptable Picloram LDUP 272108 0 Ag/L N/A ND 30 NIA 12/12/02 Acceptable %Ree Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 2 of 7 RPD Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Limit OOS-Low QC Result Below LCL LCL Lower Control Limit