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BSKANALYTICAL LABORATORIES QC Summary Report 12/30/2002 11111//II1111111[IIIII IIIII 111111111111111 OF VIII 11III 1III BSK Submission 2002120386 Client Caltest Analytical Laboratory Date Submitted 12/06/2002 Project 1D C120220 Project Desc BSK StarLuns Run# 47620 11111111111111111111111111111111111 Instrument ID GC7 Analyst Initials RACHELM Method Number 5153 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Umts or RPD RPD Cone Cone UCL LCL Date 2,4,5-T MS 272107 2 89 pg/L 95 3 04 ND 130 70 12/12/02 Acceptable 2,4,5-TP(Stivex) MS 272107 311 pg/L 103 30 ND 130 70 12/12/02 Acceptable 2,4-D MS 272107 314 pg/L 100 313 ND 130 70 12/12/02 Acceptable Bentazon(Basagran) MS 272107 564 pWL 93 606 ND 130 70 12/12/02 Acceptable Dalapon MS 272107 2834 }µg/L 94 30 1 ND 130 70 12/12/02 Acceptable Dicamba(Banvel) _ MS 272107 476 µg/L 106 446 ND 130 70 12/12/02 Acceptable Dinoseb(DNBP) MS 272107 608 ]ig/L 101 598 ND 130 70 12/12/02 Acceptable Pentachlorophenol(PCP) MS 272107 058 µg/L 96 060 ND 130 70 12/12/02 Acceptable Picloram MS 272107 277 pg/L 94 294 ND 130 70 12/12/02 Acceptable 2 4,5-T MSD 272107 283 pg/L 93 2 304 ND 130 70 12/12/02 Acceptable 2,4,5-TP(Silvex) MSD 272107 302 pg/L 100 3 30 ND 130 70 12/12/02 Acceptable 2,4-D MSD 272107 3006 pg/L 96 43 31 3 ND 130 70 12/12/02 Acceptable Bentazon(Basagran) MSD 272107 542 gg/L 89 4 606 ND 130 70 12/12/02 Acceptable Dalapon MSB 272107 2722 pg/L 90 4 301 ND 130 70 12/12/02 Acceptable Dicamba(Banvel) MSD 272107 4 5 pg/L 100 5 7 446 ND 130 70 12/12/02 Acceptable Dmoseb(DNBP) MSD 272107 588 µg/L 98 3 3 598 ND 130 70 12/12/02 Acceptable Pentachlorophenol(PCP) MSD 272107 054 µg/L 90 7 1 060 ND 130 70 12/12/02 Acceptable Picloram MSD 272107 296 gg/L 100 67 294 ND 130 70 12/12/02 Acceptable -------------------------------------- ----- 2,4,5-T RB LK NIA 0 ug/L < 1 1 NIA 12/12/02 Acceptable 2,4,5-TP(Silvex) RBLK N/A 0 pg/L < 1 1 N/A 12/12/02 Acceptable 2,4-D RBLK N/A 0 pg/L <10 10 N/A 12/12/02 Acceptable Bentazon(Basagran) RBLK N/A 0 pg/L <2 2 N/A 12/12/02 Acceptable Dalapon R13L.K NIA 0 pg/L <10 10 N/A 12/12x02 Acceptable Dicamba(Banvel) RBLK NIA 0 pg/L <1 5 1 5 N/A 12/12/02 Acceptable Dinoseb(DNBP) RBLK NIA 0 pg/L <2 2 N/A 12/12/02 Acceptable Pentachlorophenol(PCP) RBLK N/A 0 gg/L <02 0 2 N/A 12/12/02 Acceptable Picloram RBLK N/A 0 pg/L Run Comments The MSD surrogate recovery was slightly low due to probable matrix effects Surrogate Results Analyte QC Type Surr Result UCL LCL Date DCPAA LCS N/A 72 %Rec 70 130 70 12/12/02 Acceptable DCPAA LCSD N/A 73 %Rec 70 130 70 12/12/02 Acceptable DCPAA LDUP 272108 70 %Rec 75 130 70 12/12/02 Acceptable ODCPAA MS 272107 71 %Rec 74 130 70 12/12/02 Acceptable DCPAA MSD 272107 67 %Rec 74 130 70 12/12/02 OOS-Low %Rec Percent Recovered Parent Sample Sample used as background matnx for MS/MSD Page 3 of 7 RPD Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Limit OOS-Low QC Result Below LCL LCL Lower Control Limit