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BSKANALYTICAL LABORATORIES QC Summary Report 12/30/2002 BSK Submission 20021203$6 Client Caltest Analytical Laboratory Date Subtmtted 12/06/2002 Project ID 0120220 Project Desc BSK StarLtms Run# 47932 IIIIIIIIIIIIIIIIIiIIIIIIIIVIIIIII Instrument ID SVGCMS2 Analyst Initials DANB Method Number 525 Analyte Results Matrix %Ree Spike Spk Matrix Analyte QC Type Spike 11) Remit Units or RPD RPD Cone Cone UCL LCL Date Alachlor(Alanex) LCSD N/A 649 gg/L 129 20 5 ND 130 70 12/18/02 Acceptable Benw(a)pyrene LCSD N/A 206 µg/L 68 12 3 ND 130 70 12/18/02 OOS-Low bis(2-ethylhexyll adipate LCSD N/A 483 1tg/L 96 34 5 ND 130 70 12/18/02 Acceptable bis(2-ethylhexyl)phthalate LCSD N/A 522 µg/L 104 096 5 ND 130 70 12/18/02 Acceptable Butachlor LCSD NIA 43 µg/L 143 21 3 ND 130 70 12/18/02 OOS-High Diazinon LCSD N/A 557 4g/L 111 13 5 ND 130 70 12/18/02 Acceptable Metolachlor LCSD N/A 666 ltg/L 133 14 5 ND 130 70 12/18/02 OOS-High Molmate(Ordram) LCSD NIA 637 pg/L 127 20 5 ND 130 70 12/18/02 Acceptable Prometryn(Caparol) LCSD N/A 743 pg/L 148 24 5 ND 130 70 12/18/02 OOS-High Propachlor LCSD N/A 953 µg/L 190 61 5 ND 130 70 12/18/02 OOS-High Thtobencarb(Bolero) LCSD NIA 634 µg/L 126 15 5 ND 130 70 12/18/02 Acceptable --------------------------------------- -- --._----- Alachlor(Alanex} RBLK N/A 0 µg/L <1 1 NIA 12/18/02 Acceptable Atrazine(AAtrex) RBLK N/A 0 ug/L < 1 1 N/A 12/18/02 Acceptable Benzo(a)pyrene RBLK N/A 0 µg/L <01 0 1 NIA 12/18/02 Acceptable bis(2-ethylhexyl)adipate R13LK N/A 0 µg/L <3 3 N/A 12/18/02 Acceptable bis(2-ethylhexyl)phthalate R13LK N/A 0 µg/L <3 3 N/A 12/18/02 Acceptable Bromacil(Hyvar) RBLK NIA 0 pg/L < to 10 N/A 12/18/02 Acceptable Butachlor RBLK N/A 0 µg/L <038 0 38 N/A 12/18/02 Acceptable Diazinon RBLK N/A 0 µg/L <025 0 25 N/A 12/18/02 Acceptable Dtmethoate(Cygon) RBLK N/A 0 µg/l- <10 10 N/A 12/18/02 Acceptable Metolachlor RBLK N/A 0 µg/L <05 0 5 N/A 12/18/02 Acceptable Metnbuzin RBLK N/A 0 µg/L <05 0 5 N/A 12/18/02 Acceptable Molmate(Ordram) R13LK N/A 0 µg/L <2 2 N/A 12/18/02 Acceptable Prometryn(Caparol) RBLK NIA 0 µg/L <2 2 N/A 12/18/02 Acceptable Propachlor RBLK NIA 0 µg/L <05 0 5 N/A 12/18/02 Acceptable Stmazme(Prmcep) RBLK N/A 0 µg/L < 1 1 NIA 12/18/02 Acceptable Thiobencarb(Bolero) RBLK N/A 0 µg/L <1 1 N/A 12/18/02 Acceptable Run Comments LCSD recoveries were out of range however the LCS recoveries were within the acceptance ranges Surrogate Results Analyte QC Type Surr Result UCL LCL Date 1,3-Dimethyl-2-nitrobenzene LCS N/A 1084 %Rec 100 130 70 12/18/02 Acceptable 1,3-Dimethyl-2-nitrobenzene LCSD NIA 23 4 %Rec 100 130 70 12/18/02 ODS-Low --,—� — -------— --------.—-------------------- 1,3-Dimethyl-2-nitrobenzene RBLK N/A—— —10-0 5 %Rec 130 70 12/18/02 Acceptable c� %Rec Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 5 of 7 RPR Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Ltmtt OOS-Low QC Result Below LCL LCL Lower Control Limit