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BSKANALYTICAL LABORATORIES QC Summary Report 12/30/2002 11111[llli111111111111111Illlllllllllllllllllllllfllllllllll BSK Submission 2002120386 Client Caltest Analytical Laboratory Date Submitted 12/06/2002 Project 1D C120220 Project Desc BSK StarLinis Run# 48121 11111111 111111111 Instrument ID SVGCMSI Analyst Initials DANB Method Number 548 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Conc Conc UCL LCL Date Endothall LCS N/A 617 pg/L 61 100 ND 150 50 12/23/02 Acceptable Endothall LCSD N/A 577 pg/L 57 68 100 ND 150 50 12/23/02 Acceptable Endothall MS 272992 132 gg/L 83 100 ND 150 50 12/23/02 Acceptable ------------------- --------------------------- N/A _._._. — ---------------------- N/A 0 pg/L <45 45 N/A 12/23/02 Acceptable BSK StarLims Run# 48292 11111111iiiiii1111111111illifilllu Instrument ID HPLC1 Analyst Initials TIMC Method Number 531 1 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Conc Conc UCL LCL Date 3-Hydroxycarbofuran LCS N/A 307 pg/L 102 30 ND 130 70 12/22/02 Acceptable Aldicarb LCS N/A 314 pg/L 104 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfone LCS NIA 299 pg/L 99 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfoxide LCS N/A 310 pg/L 103 30 ND 130 70 12/22/02 Acceptable Carbaryl LCS N/A 300 pg/L 100 30 ND 130 70 12/22/02 Acceptable Carbofuran LCS NIA 299 pg/L 99 30 ND 130 70 12/22/02 Acceptable Methomyl LCS N/A 315 pg/L 105 30 ND 130 70 12/22/02 Acceptable Oxamyl LCS N/A 310 pg/L 103 30 ND 130 70 12/22/02 Acceptable 3-Hydroxycarbofuran LCSD N/A 318 pg/L 106 36 30 ND 130 70 12/22/02 Acceptable Aldicarb LCSD N/A 300 pg/L 100 46 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfone LCSD N/A 297 pg/l- 99 068 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfoxide LCSD N/A 299 gg/L 99 37 30 ND 130 70 12/22/02 Acceptable Carbaryl LCSD N/A 285 pg/L 95 5 1 30 ND 130 70 12/22/02 Acceptable Carbofuran LCSD N/A 293 gg/L 97 2 30 ND 130 70 12/22/02 Acceptable Methomyl LCSD N/A 304 pg/L 101 36 30 ND 130 70 12/22/02 Acceptable Oxamyl LCSD N/A 314 pg/L 104 12 30 ND 130 70 12/22/02 Acceptable 3-Hydroxycarbofuran MS 270066 319 pg/L 106 30 ND 130 70 12/22/02 Acceptable Aldicarb MS 270066 320 gg/L 106 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfone MS 270066 302 pg/I. 100 30 ND 130 70 12/22/02 Acceptable Aldicarb Sulfoxide MS 270066 308 pg/L 102 30 ND 130 70 12/22/02 Acceptable Carbaryl MS 270066 308 µg/L 102 30 ND 130 70 12/22/02 Acceptable Carbofuran MS 270066 307 gg/L 102 30 ND 130 70 12/22/02 Acceptable Methomyl MS 270066 305 pg/L 101 30 ND 130 70 12/22/02 Acceptable Oxamyl MS 270066 309 pg/L 103 30 ND 130 70 12/22/02 Acceptable 3-Hydroxycarbofuran RBLK N/A 0— gg/L <3 F—— 3 N/A 12/22/02~Acceptable +• Aldicarb RBLK NIA 0 pg/L <3 3 N/A 12/22/02 Acceptable %Rec Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 6 of 7 RPL) Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Linut OOS-Law QC Result Below LCL LCL Lower Control Limit