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BSKA NA L Y T I C A L LABORATORIES Charlya Heang Certificate of Analysis Caltest Analytical Laboratory FLAP Certificate #1180 1885 N Kelly Road Report Issue Date 09/30/2002 Napa, CA 94558 BSK Submission #: 2002090292 BSK Sample ID#. 245597 Project ID C090158 Project Desc Submission Continents Sample Type Liquid Date Sampled 09/05/2002 Sample Description Effluent Flag Clay Time Sampled I310 Sample Comments Date Received 09/06/2002 Organics Prep Analysis Analyte Method Result Units MDL ML Dilution DLR Date Date Dibromochloropropane EPA 504 1 NO gg/L 0 007 001 1 001 09/12/2002 09/14/2002 Ethylenedibronude EPA 504 1 NO pg/l, 0 004 002 1 002 09/12/2002 09/14/2002 2,4,5-TP(Silvex) EPA 515 3 NO µg/L 042 1 0 1 10 09/09/2002 09/10/2002 2,4-D EPA 5I5 3 NO µg/L, 53 10 1 10 09/09/2002 09/10/2002 Bentazon(Basagran) EPA 515 3 NO µg/L 084 20 1 2 09/09/2002 09/10/2002 Dalapon EPA 515 3 2 06 DNQ µg/L 1 6 10 1 10 09/09/2002 09/10/2002 Dinoseb(DNBP) EPA 515 3 NO pg/L 049 20 1 2 09/09/2002 09/10/2002 Pentachlorophenol(PCP) EPA 515 3 0 02 DNQ pg/L 002 02 1 02 09/09/2002 09/10/2002 Picloram EPA 515 3 NO µg/L, 027 1 0 1 1 09/09/2002 09/10/2002 Alachlor(Alanex) EPA 525 2 ND pg/L 03 to 1 1 09/13/2002 09/16/2002 Atrazine(AAtrex) EPA 525 2 NO µg/L. 08 10 1 1 09/13/2002 09/16/2002 bis(2-ethylhexyl)adipate EPA 525 2 NO gg/L 051 30 1 3 09/13/2002 09/16/2002 Diazinon EPA 525 2 ND pg/L 0 10 025 1 025 09/13/2002 09/16/2002 Molinate(Ordram) EPA 525 2 NO µg/L 028 20 1 2 09/13/2002 09/16/2002 Simazine(Pnncep) EPA 525 2 NO µg/1. 038 10 1 1 09/13/2002 09/16/2002 Thiobencarb(Bolero) EPA 525 2 ND pg/L 045 10 1 1 09/13/2002 09/16/2002 Carbofuran EPA 531 1 ND µg/L 1 3 50 1 50 09/21/2002 09/21/2002 Oxamyl EPA 531 1 NO lig/l, 26 200 1 20 09/21/2002 09/21/2002 Glyphosate EPA 547 NO pg/L 46 25 1 25 09/19/2002 09/24/2002 Diquat EPA 549 1 NO pg/L. 08 4 1 4 09/11/2002 09/18/2002 Surrogate - - - - - - --- -- - ----- - - - ---- ---- - -- - - ---- Bromoform -- -- - - ------ - - -- - - -- - EPA 504 1 1110 %Rec - I N/A 09/12/2002 09/14/2002 DCPAA EPA 515 3 86 %Rec 1 N/A 09/09/2002 09/10/2002 DNQ=Detected,not quantified The trace values between the MDL and DLR are of an unknown data quality Baseline noise, calibration curve extrapolation below the lowest calibrator,method blank detections,and integration artifacts can all produce apparent DNQ values,which contribute to the un-reliability of these values mg/L, M3111grams/Liter(ppm) MDL Method Detection Lima H Analyzed outside of hold time 0 mg/Kg Mtlhgrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result Ng/L Micrograms/Liter(ppb) PQL x Dilution µg/Kg Micrograms/Kilogram(ppb) ND None Detected above MDL S Suspect result See Cover Letter for comments ML Practical Quantitation Limit E Analysis performed by Extemal laboratory %Rec Percent Recovered(surrogates) See External Laboratory Report attachments DNQ Detected,Not Quantified DNQ Trace Result(>MDL, DLR) Trace results are only qualitative values(estimates) Report Authentication Code 1111111011111111111111101111111111 filial 011011111119 liII IIfll11111111 Page ] of 2 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559485-6935