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BSKANA L Y T I C A L <br /> LABORATORIES <br /> s <br /> Charlya Heang Certificate of Analysis <br /> Caltest Analytical Laboratory ELAP Certificate 41180 <br /> 1885 N Kelly Road Report Issue Date 09/30/2002 <br /> Napa, CA 94558 <br /> BSK Submission##: 2002090292 <br /> BSK Sample ID#: 245597 <br /> Project lD C090158 Project Desc <br /> Submission Comments <br /> Sample Type Liquid Date Sampled 09/05/2002 <br /> Sample Description Effluent Flag City Time Sampled I310 <br /> Sample Comments Date Received 09/06/2002 <br /> Organics <br /> Prep Analysis <br /> Analyte Metbod Result Units MDL ML Dilution ALR Date Date <br /> 1,3-Dimethyl-2-nitrobenzene EPA 525 2 100 %Rec 1 N/A 09/13/2002 09/16/2002 <br /> BDMC EPA 531 1 74 %Rec 1 N/A 09/21/2002 09/21/2002 <br /> AMPA EPA 547 928 %Ree - 1 N/A 09/19/2002 09/24/2002 <br /> DNQ=Detected,not quantified The trace values between the MDL and DLR are of an unknown data quality Baseline noise, <br /> calibration curve extrapolation below the lowest calibrator,method blank detecttons, and integration artifacts can all produce apparent <br /> DNQ values,which contnbutc to the un-reliability of these values <br /> mg/L Milligrams:/Liter(ppm) MDL Method Detection Limit H Analyzed outside of hold time <br /> . mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P preliminary result <br /> µg/L Micmgranis/Liter(ppb) PQL x Dilution <br /> i-ams/Ktlogram{ppb) ND None Detected above MDL S Suspect result See Cover Letter for comments <br /> µg/Kg Mtcrog <br /> %Rec Percent Recovered(surrogates) ML Practical Quantitation Unut E Analysis performed by External laboratory <br /> See External Laboratory Report attachments <br /> DNQ Detected,Not Quantified DNQ Trace Result(>MDL, DLR) Trace results are only qualitative values(estimates) <br /> Report Authentication Code 11H1111111111E1111111111u111IN1111111111MN1111191911111i11111111111 Page 2of2 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />