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4 BSKANALYTICAL LABORATORIES • QC Summa Report ep ort 10/01X2002 1111111 VIII!fill Iflll Ill/!IIIA VIII!1111!1111 lIII111111III BSK Sabnussion 2002090292 Client Caltest Analytical Laboratory Date Submitted 09/06/2002 Prosect ID C090158 Prosect Desc BSK StarLlms Run #• 43037 Illlflllilllllllllflllllllllfllllll Instru lent 1D GC7 Ana]Yst Initials. RACHELM Method Number 5153 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Cone Cone UCL LCL Date 2,4,5-T LCs N/A 339 gg/L 111 304 ND 130 70 09/I0/02 Acceptable 2,4,5-TP(Silvex) LCS NIA 327 pg/L 109 30 ND 130 70 09/10/02 Acceptable 2,4-D LCS NIA 2999 pg/L 95 31 3 ND 130 70 09/10/02 Acceptable Bentazon(Basagran) LCS NIA 576 pg/L 95 606 ND 130 70 09/10/02 Acceptable Dalapon LCS NIA 297 gg/L 98 30 1 ND 130 70 09/10/02 Acceptable Dicamba(Banvel) LCS N/A 414 gg/L 92 446 ND 130 70 09/10/02 Acceptable Dinoseb(DNBP) LCS N/A 623 gg/L 104 598 ND 130 70 09/10/02 Acceptable Pentachlorophenol(PCP) LCS N/A 062 lig/L, 103 060 ND 130 70 09/10/02 Acceptable Picloram LCS NIA 331 pg/L 112 294 ND 130 70 09/10/02 Acceptable 2,4,5-T LCSD NIA 338 pg/L 111 029 304 ND 130 70 09/10/02 Acceptable 2,4,5-TP(Silvex) LCSD N/A 333 pg/L 1 I 1 19 30 ND 130 70 09/10/02 Acceptable 2,4-D LCSD N/A 2815 gg/L 89 63 313 ND 130 70 09/10/02 Acceptable Bentazon(Basagran) LCSD N/A 543 pg/L 89 59 606 ND 130 70 09/10/02 Acceptable Dalapon LCSD N/A 28 13 pg/L 93 54 30 1 ND 130 70 09/10/02 Acceptable Dicamba(Banvel) LCSD N/A 389 pg/L 87 62 446 ND 130 70 09/10/02 Acceptable Dinoseb(DNBP) LCSD N/A 631 pg/L 105 12 599 ND 130 70 09/10/02 Acceptable Pentachlorophenol(PCP) LCSD N/A 063 µ8/L 105 17 060 ND 130 70 09/10/02 Acceptable Picloram LCSD N/A 329 pg/L ill 061 294 ND 130 70 09/10/02 Acceptable 2,4,5-T MS 243873 315 pg/L 103 304 ND 130 70 09/10/02 Acceptable 2,4,5-TP(Silvex) MS 243873 3 03 pg/L 101 300 ND 130 70 09/10/02 Acceptable 2,4-D MS 243873 2732 pg/L 87 31 3 ND 130 70 09/10/02 Acceptable Bentazon(Basagran) MS 243873 531 pg/L 87 606 ND 130 70 09/10/02 Acceptable Dalapon MS 243873 2875 pg/L 95 30 1 ND 130 70 09/10/02 Acceptable Dicamba(Banvel) MS 243873 392 pg/L 85 446 ND 130 70 09/10/02 Acceptable Dinoseb(DNBP) MS 243873 584 pg/L 97 598 ND 130 70 09/10/02 Acceptable Pentachlorophenol(PCP) MS 243873 058 gg/L 96 060 ND 130 70 09/10/02 Acceptable Picloram MS 243873 302 pg/L 102 294 ND 130 70 09/10/02 Acceptable 2,4,5-1 MSD 243873 32 pg/L 105 16 304 ND 130 70 09/10/02 Acceptable 2,4,5-TP(Silvex) MSD 243873 32 gg/L 106 54 300 ND 130 70 09/10/02 Acceptable 2,4-D MSD 243873 2677 pg/L 85 2 31 3 ND 130 70 09/10/02 Acceptable Bentazon(Basagran) MSD 243873 524 pg/L 86 13 606 ND 130 70 09/10/02 Acceptable Dalapon MSD 243873 2691 gg/L 89 67 301 ND 130 70 09/10/02 Acceptable Dicamba(Banvel) MSD 243873 37 pg/L 82 31 446 ND 130 70 09/10/02 Acceptable Dinoseb(DNBP) MSD 243873 579 pg/L, 96 086 598 ND 130 70 09/10/02 Acceptable Pentachlorophenol(PCP) MSD 243873 059 pg/L 98 18 060 ND 130 70 09/10/02 Acceptable Picloram —a—_—— MSD — 243873 __ 31 pg/l, __105 27 294 ND _ 130 70 09/10/02 Acceptable 2,4,5-T IZBLK NIA 0 pg/L <1 1 NIA 09/10/02 Acceptable %Rec Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 1 of 6 RPD Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Limit OOS-Law QC Result Below LCL LCL Lower Control Limit