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BSKANA L Y T I C A L LABORATORIES Chanya Heang Certificate of Analysis Caltest Analytical Laboratory ELAP Certificate#1180 1885 N. Kelly Road Report Issue Date 10/11/2002 Napa, CA 94558 BSK Submission#: 2002090292 BSK Sample ID#: 245597 Project ID C090158 Project Desc Submission Comments Sample Type Liquid Date Sampled 09/05/2002 Sample Description Effluent Flag City Time Sampled 1310 Sample Comments Date Received 09/06/2002 Organics Prep Analysis Analyte Method Result Units MDL ML Dilution DLR Date Date Dibromochioropropane EPA 504 1 NO pg/L 0 007 001 1 001 09/12/2002 09/14/2002 Ethylenedibromide EPA 504 1 NO µg/l- 0 004 002 1 002 09/12/2002 09/14/2002 2,4,5-TP(Silvex) EPA 515 3 NO µg/l- 042 10 1 10 09/09/2002 09/10/2002 2,4-D EPA 515 3 NO µg/L 5 3 10 1 10 09/09/2002 09/10/2002 Bentazon(Basagran) EPA 515 3 NO µg/L 084 20 1 2 09/09/2002 09/10/2002 �T Dalapon EPA 515 3 2 06 DNQ µg/L 1 6 10 1 10 09/09/2002 09/10/2002 Dtnoseb(DNBP) EPA 515 3 NO pg/L 049 20 1 2 09/09/2002 09/10/2002 Pentachlorophenol(PCP) EPA 515 3 0 01 DNQ pg/L 002 02 1 02 09/09/2002 09/10/2002 �- Picloram EPA 515 3 NO pg/L 027 10 1 1 09/09/2002 09/10/2002 Alachlor(Alanex) EPA 5252 NO µg/L 03 10 1 1 09/13/2002 09/16/2002 Atrazine(AAtrex) EPA 525 2 NO µg/L 08 10 1 1 09/13/2002 09/16/2002 bis(2-ethylhexyl)adipate EPA 525 2 NO µg/L 051 30 1 3 09/13/2002 09/16/2002 Diazinon EPA 525 2 NO pg/L 0 10 025 1 025 09/13/2002 09/16/2002 Mohnate(Ordram) EPA 525 2 ND pg/L 028 20 1 2 09/13/2002 09/16/2002 Sunazine(Pnncep) EPA 525 2 NO pg/L 038 10 1 1 09/13/2002 09/16/2002 Thiobencarb(Bolero) EPA 525 2 NO µg/L 045 10 1 1 09/13/2002 09/16/2002 — Carbofuran EPA 531 1 ND µ&/L 1 3 so 1 50 09/21/2002 09121/2002 Oxamyl EPA 531 1 NO µg/L 26 200 1 20 09/21/2002 09/21/2002 Glyphosate EPA 547 ND pg/L 46 25 1 25 09/19/2002 09/24/2002 -- Endothall EPA 548 1 NO }ig/L 19 45 1 45 09/10/2002 09/18/2002 �- Diquat EPA 549 1 ND µg/L 08 4 1 4 09/11/2002 09/18/2002 Surrogate -------------------------------------------------------- Bromofonn EPA 504 1 1110 %Rec - 1 N/A 09/12/2002 09/14/2002 DNQ=Detected,not quantified The trace values between the MDL and DLR are of an unknown data quality Baseline noise, calibration curve extrapolation below the lowest calibrator,method blank detections,and integration artifacts can all produce apparent DNQ values,which contribute to the un-reliability of these values mg/L Milligrams/Liter(ppm) MDL Method Detection Limit 11 Analyzed outside of hold time . mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result pg/L Micrograms/Liter(ppb) PQL x Dilution ND None Detected above MDI S Suspect result See Cover Letter for comments µg/Kg Micrograms/Kilogram(ppb) E Analysis performed b ML Practical Quanntation Limit Y Pe y External laboratory %Rec Percent Recovered(surrogates) See External Laboratory Report attachments DNQ Detected,Not Quantified DNQ Trace Result(>MDL,<DLR Trace results are only qualitative values(estimates) Report Authentication Code 1911118111111plll9111111M I1111111MIlflEll1111111so11091 page 1 oft 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935