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BSKANALYTICAL <br /> LABORATORIESI <br /> Chanya Heang Certificate of Analysis <br /> Caltest Analytical Laboratory ELAP Certificate#1180 <br /> 1885 N. Kelly Road Report Issue Date 10/11/2002 <br /> Napa, CA 94558 <br /> BSK Submission##: 2002090292 <br /> BSK Sample ID ## 245597 <br /> Project ID C090158 Project Desc <br /> Submission Comments <br /> Sample Type Liquid Date Sampled 09/05/2002 <br /> Sample Description Effluent Flag City Time Sampled 1310 <br /> Sample Comments Date Received 09/06/2002 <br /> Organics <br /> Prep Analysts <br /> Analyte Method Result Units MDL ML Dilution DLR Date Date <br /> DCPAA EPA 515 3 86 %Rec 1 N/A 09/09/2002 09/10/2002 <br /> 1,3-Dimethyl-2-nitrobenzene EPA 525 2 100 %Rec I NIA 09/13/2002 09/16/2002 <br /> BDMC EPA 531 1 74 %Rec - 1 NIA 09/21/2002 09/21/2002 <br /> AMPA EPA 547 928 %Rec - 1 NIA 09/19/2002 09124!2002 <br /> DNQ=Detected,not quantified The trace values between the MDL and DLR are of an unknown data quality Baseline noise, <br /> calibration curve extrapolation below the lowest calibrator,method blank detections, and integration artifacts can all produce apparent <br /> DNQ values,which contribute to the un-reliability of these values <br /> mg(L Mtlligmms/Liler(ppm) MDL Method Detection Limit H Analyzed outside ofhold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Luna for Reporting P Preliminary result <br /> 1ig1L Micrograms/Liter(ppb) PQL x Dilution 5 Suspect result See Cover Letter for comments. <br /> pg/Kg Mwrograrns/Kdogram(ppb) ND None Detected above MDI E sis AnalY <br /> ML Practical Quantitation Limit performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> DNQ Detected,Not Quantified DNQ Trace Result(>MDI„<DLR Trace results are only qualitative values(estimates) <br /> Repm Authentication Code 111313111111111N111M1111110111111 UH I IM1011191011E111H Page 2 of 2 <br /> 1414 Stantslaus Street Fresno,CA 93706-1623 Phone 559497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />