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McCampbell Analytical .Inc <br />1 <br />110 2nd Avenue South, #D7 Pacheco CA 94553-5560 <br />Telephone 925-798-1620 Fax 925-798-1622 <br />L httpJ/www mecampbell corn E-mail main@mecampbell cam <br />Advanced GeoEnvironmental, Inc <br />837 Shaw Road <br />Stockton, CA 95215 <br />Client Project ID Flag City Chevron <br />Date Sampled 06/14/02 <br />Date Received 06/18/02 <br />Client Contact Tun Cuellar <br />Date Extracted 06117/02-06/18/02 <br />Client P O <br />Date Analyzed 06/18/02-06/21/02 <br />Diesel (C] 0-23) and Oil (CIS+) Range Extractable Hydrocarbons as Diesel and Motor Od* <br />traction method SW3510C Analytical methods SW8015C Work Order 0206271 <br />Lab ID <br />Client ID <br />Madix <br />TPH(d) <br />TPH(mo) <br />DF <br />% SS <br />0206271-001B <br />MW5/061402 <br />W <br />ND <br />ND <br />1 <br />113 <br />0206271-002B <br />MW7/061402 <br />W <br />ND <br />ND <br />1 <br />112 <br />0206271-003B <br />MWlla/061402 <br />W <br />ND <br />ND <br />1 <br />112 <br />0206271-00413 <br />MWllb/061402 <br />W <br />ND <br />ND <br />1 <br />114 <br />0206271-005B <br />MWlle/061402 <br />W <br />87,b,f <br />ND <br />1 <br />111 <br />0206271-006B <br />MWlld/061402 <br />W <br />89,b,f <br />ND <br />I <br />108 <br />0206271-007B <br />MW12a/061402 <br />W <br />430,b,g <br />350 <br />1 <br />---# <br />0206271-008B <br />MW12b/061402 <br />W <br />100,b,f <br />ND <br />1 <br />948 <br />0206271-009B <br />MW12c/061402 <br />W <br />72,b,f <br />ND <br />1 <br />934 <br />0206271-010B <br />MW12d/061402 <br />W <br />83,b,f <br />ND <br />1 <br />113 <br />020627I-011B <br />MW13a/061402 <br />W <br />81,b,f <br />ND <br />1 <br />112 <br />0206271-0128 <br />MWl3b/061402 <br />W <br />95,b,f <br />ND <br />1 <br />113 <br />0206271-013B <br />MW13c/061402 <br />W <br />75,b,f <br />ND <br />1 <br />113 <br />0206271-014B <br />MW13d/061402 <br />W <br />69,b,f <br />ND <br />L <br />115 <br />Reporting Limit for DF =1, <br />ND means not detected at or <br />above the reporting limit <br />W <br />50 <br />250 <br />µg/L <br />S <br />NA <br />NA <br />mg/Kg <br />* water and vapor samples are reported in ug/L, wipe samples to ug/wipe, soil and sludge samples in mg/kg, and all TCLP / STLC / SPLP extracts in <br />ug/L <br /># cluttered chromatogram resulting in coeluted surrogate and sample peaks, or, surrogate peak is on elevated baseline, or, surrogate has been <br />diminished by dilution of original extract <br />+The follovwing descriptions of the TAH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation a) <br />unmodified or weakly modified diesel is significant, b) diesel range compounds are significant, no recognizable pattern, c) aged diesel" is significant), <br />d) gasoline range compounds are significant, e) unknown medium boiling point pattern that does not appear to be derived from diesel, f) one to a few <br />isolated peaks present, g) oil range compounds are significant, h) lighter than water immiscible sheen/product is present, i) liquid sample that contains <br />greater than --2 vol % sediment, k) kerosene/kerosene range, 1) bunker oil, m) fuel oil, n) stoddard solvent <br />I <br />DHS Certification No 1644 <br />Edward Hamilton, Lab Director <br />