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• <br />110 2nd Avenue South #D7 Pacheco, CA 94553-5560 <br />McCarnpbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br />Advanced GeoEnvtronmental, Inc <br />837 Shaw Road <br />Stockton, CA 95215 <br />Client Project ID Flag City Chevron <br />Date Sampled 06/14/02 <br />Date Received 06/18/02 <br />Client Contact Tim Cuellar <br />Date Extracted 06/21/02-06122/02 <br />Client P O <br />Date Analyzed 06/21/02-06/22/02 <br />Oxygenated Volatile Organics by GC/MS* <br />Extraction Method SW5030B Analytical Method SW8260B Work Order 0206271 <br />Lab ID <br />0206271-OOIC <br />0206271-002C 0206271-003C <br />0206271-004C <br />Client ID <br />MW5/061402 MW7/061402 MW11a/06t402 <br />MW1lb/061402 <br />Reporting Limit for <br />Matrix <br />W i W i W <br />W <br />DF =1 <br />DF <br />1 i 2 1 <br />33 <br />S <br />W <br />Compound <br />Concentration <br />ugIkg <br />µg/l. <br />Dusopropyl ether (RIPE) <br />ND <br />ND<l <br />ND <br />ND<l 7 <br />NA <br />05 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />ND<l <br />ND <br />ND<1 7 <br />NA <br />05 <br />Methyl -t -butyl ether (MTBE) <br />ND <br />49 <br />1 0 <br />120 <br />NA <br />05 <br />tert-Amyl methyl ether (TAME) <br />ND <br />ND<I <br />ND <br />ND<l 7 <br />NA <br />05 <br />t -Butyl alcohol (TBA) <br />ND <br />ND<10 <br />ND <br />ND<17 <br />NA <br />50 <br />Methanol <br />ND <br />ND<1000 <br />ND <br />ND<1700 <br />NA <br />500 <br />Ethanol <br />ND <br />ND<100 <br />ND <br />ND<170 <br />NA <br />50 <br />1,2-Dibromcethane (EBB) <br />ND <br />ND<1 <br />ND <br />ND<l 7 <br />NA <br />05 <br />1,2-Dichloroethane (1,2 -DCA) <br />ND <br />ND<1 <br />ND <br />ND<l 7 <br />NA <br />05 <br />Surrogate Recoveries (%) <br />%SS 974 <br />101 <br />100 <br />102 <br />Comments <br />* water samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / STLC I SPLP extracts in ug/L <br />ND means not detected above the reporting limit, N/A means surrogate not applicable to this analysis <br />(h) lighter than water immiscible sheen/product is present, (i) liquid sample that contains greater than —2 vol % sediment, 0) sample diluted due to high <br />organic content <br />DHS Certification No 1644 <br />Edward Hamilton, Lab Director <br />