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• <br />• <br />McCampbell Analytical Inc <br />110 2nd Avenue South, #D7, Pacheco, CA 94553-5560 <br />Telephone 925-798-1620 Fax 925-798-1622 <br />http //www in=rnpbell cum F mad mam@mccampbell cam <br />Advanced GeoEnvlronmental, Inc <br />837 Shaw Road <br />Stockton, CA 95215 <br />Client Project ID Flag City Chevron <br />Date Sampled 06/14/02 <br />Date Received 06/18/02 <br />Client Contact Tim Cuellar <br />Date Extracted 06121/02-06122102 <br />Client P O <br />Date Analyzed 06121102-06/22/02 <br />F-Mracnon Method SW5030B <br />Oxygenated Volatile Organics by GC/MS* <br />Analytical Method SW8260B Work Order 0206271 <br />Lab ID <br />0206271-005C j 0206271-006C 10206271-007C <br />0206271-008C <br />Client ID <br />MWI1d061402 <br />MWI1d/061402 j MW12a/061402 <br />MW12b/061402 <br />Reporting Linut for <br />Matrix <br />W <br />W W <br />W <br />DF =1 <br />DF <br />1 1 i 1 <br />1 <br />S <br />W <br />Compound <br />Concentration <br />ug/kg <br />µg/I <br />Dusopropyl ether (DIPE) <br />ND <br />ND <br />ND <br />ND <br />NA <br />05 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />ND <br />ND <br />ND <br />NA <br />05 <br />Methyl -t -butyl ether (MTBE) <br />ND <br />72 <br />56 <br />ND <br />NA <br />05 <br />tert-Amyl methyl ether (TAME) <br />ND <br />ND <br />ND <br />ND <br />NA <br />05 <br />t -Butyl alcohol (FBA) <br />ND <br />ND <br />ND <br />ND <br />NA <br />50 <br />Methanol <br />ND <br />ND <br />ND <br />ND <br />NA <br />500 <br />Ethanol <br />ND <br />ND <br />ND <br />ND <br />NA <br />50 <br />1,2-Dibromoethane (EDB) <br />ND <br />ND <br />ND <br />ND <br />NA <br />05 <br />1,2-Dichloroethane (1,2 -DCA) <br />ND <br />ND <br />ND <br />ND <br />NA <br />05 <br />Surrogate Recoveries (%) <br />%SS <br />994 <br />101 <br />102 <br />967 <br />Comments <br />" water samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP / STLC / SPLP extracts in ug/L <br />ND means not detected above the reporting limit. N/A means surrogate not applicable to this analysis <br />(h) lighter than water immiscible shcen/product is present, (i) liquid sample that contains greater than —2 vol % sediment, {1) sample diluted due to high <br />organic content <br />DHS Certification No 1644 <br />Edward Hamilton, Lab Director <br />