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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC 'T'elephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail rnarn@mccampbell com <br /> Advanced GeoEnviromnxental Client Project ID Flag City Chevron Date Sampled 03/03/2001 <br /> 837 Shaw Road Date Received 03/13/2001 <br /> Stockton, CA 95215 Chent Contact Tun Cuellar Date Extracted 03/14-03/1512001 <br /> Client P O Date Analyzed 03/14-0311512001 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 62468 62469 62470 62471 <br /> MW8A/3�- MWSB/3�- MW8C/3- MW9A/3- Reporting Limit <br /> Ghent ID 09-01 09-01 09-01 09-01 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND ND<10 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND ND<10 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 680 50 10 <br /> tert-Amyl Methyl Ether(TAME) NO ND ND ND<10 50 10 <br /> tert-Butanol ND ND ND ND<50 25 50 <br /> IMethanol ND ND ND ND<2000 1000 200 <br /> Ethanol ND ND ND N17<500 250 50 <br /> Surrogate Recoveries <br /> IDibromo fluoromethane 107 107 107 107 <br /> IComments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to ug/wipe and all TCLP/$TLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water inuniscible sheen is present,(t)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />