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I <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Nip//www mccarnpbelI com E-mail matn@mccampbell cam <br /> t� <br /> Advanced GeoEtivtronmental Client Project ID Flag City Chevron Date Sampled 03/09/2001 <br /> 837 Shaw Road Date Received 03/13/2001 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 03/14-0311512001 <br /> Client P O Date Analyzed 03/14-03/15/2001 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 62472 62473 62474 62475 <br /> MW9B/3- MW9C/3-� MWIIA/3- MW11B/3- ReportingLrmit <br /> Client ID 09-01 09-01 09-01 09-01 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Dt-isopropyl Ether(DIPS) ND ND NIK5 0 ND<10 50 to <br /> Ethyl tent-Butyl Ether(ETBE) ND ND ND<5 0 ND<10 50 10 <br /> IMethyl-tert Butyl Ether(MTB$) ND 13 210 240 50 10 <br /> 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<5 0 NDX 10 50 10 <br /> Itert-Butanol ND ND ND<25 ND<50 25 5 0 <br /> IMethanol ND ND ND<1000 ND<2000 1000 200 <br /> IEthanol ND ND ND<250 ND<500 250 50 <br /> Surrogate Recoveries{%) <br /> IDibrornofluoromethane 106 108 108 108 <br /> IComments <br />' *water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in uglL <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water mirmscible sheen is present,(0 liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br />' high organic content <br /> DHS Certification No 1644 Edward Harnilton, Lab Director <br />