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r <br /> 110 Second Avenue South,4D7, Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br /> 24 htt :/hvww.niccam belf.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID. Flag City Chevron Date Sampled: 09/22/97 <br />' 1803 West March Lane,Ste A <br /> Date Received: 09/24/97 <br /> Stockton, CA 95207 Client Contact::Tim Cuellar Date Extracted: 09/26-09/30/97 <br />' Client P.O: Date Analyzed: 09/26-09/30/97 <br /> Volatile Organics By CC/MS <br /> EPA method 8260 <br />' Lab ID 81104 <br /> Client ID P10121-25m <br /> Matrix W <br /> Compound Concentration's Compound Concentration* <br />' Acetone` ND<4.5 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide` ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochioromethane ND Hexachlorobutadiene ND <br />' Bromodichloromethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> B70m011lethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br /> sec-Butyl benzene ND methylene Chloride... ND <br /> Pert-Butyl benzene ND Methyl ethyl ketone"' ' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone' ' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(IMTBE) --- <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene" ND <br /> Chloroform ND 1,1,1,2 Tetrachloroethane ND <br /> Chloromethane ND 1.1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 1.2,3-Trichlorobenzene ND <br /> I 1,2-Dibromo-3-chloropropane ND 12,4-Trich3orobenzenc ND <br /> Dibromomethane ND 1,1.1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1.1.2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorolluoromethane ND <br /> Dichlorodifluoromethane ND 1.23-Trichloropropanc ND <br /> 1,1-Dichloroethane ND 1.2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1.3.5-Trimethylbenzene ND <br /> ],I-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"" ND <br /> trans-1,2-Dichloroethene ND Xylenes,total "" ND <br /> 1,2-Dichloropropane ND Comuents:i <br /> 1,3-Dichloropropane ND Surrogate Recoveries('%) <br /> 2,2-Dichloropropane ND Dibromolluoromethanc 96 <br /> 1,1-D i ch loropropene ND Toluened894 <br /> cis-1,3-Dicliloropmpene ND 4-Bromotluarrobcnzene 84 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TC-LP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:Nvater samples 1 ug/L;vapor satltples 0.5 ue/L;solid and sludge samples 5 ug/kg;wipes 0.2uo/wipe <br /> I ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene-, (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chlorocthenc;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 f/Edward Hamilton, Lab Director <br />