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r <br /> 110 Second Avenue South,#D7, Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br /> http://www.mecamlabell.com E-mail: main@mecampbe11.com <br /> Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/22/97 <br />' 1803 West March Lane, Ste A <br /> Date Received: 09/24/97 <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/26-09130/97 <br />' Client P.O: Date Analyzed: 09/26-09/30/97 <br /> Volatile Organics By GC/117S <br /> EPA method 8260 <br />' Lab ID 81105 <br /> Client 1D P10/51-55m <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone" ND<4.5 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibronli(;c' ' N1) <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br />' Bromodichloromethane ND lodoinethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br /> sec-Butyl benzene ND Methylene Chloride" ND <br /> tert-Butyl benzene ND Methyl ethyl ketone"' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone` " ND <br /> Carbon Tetrachloride ND Methyl Cert-Butyl Ether(MTBE) - <br /> Chlorobenzene ND Napthalcne ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Sn,rene"' ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br />' Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene""' ND <br /> Dibromochloromethane ND 1,2.3-Trichlorobenzene ND <br /> 1,2-13ibronto-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichiomethane ND <br /> 1,2-Dichlorobenzene ND 1,1.2-Trichloroeth2ne ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2.3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzenc ND <br /> 1,2-Dichloroethane ND 1,35-Trimetlhylbenzene ND <br /> 1,1-Die1110T0etbene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroetltene ND Vinyl Chloride"' ND <br /> trans-1,2-Dichloroethene ND Xvlenes,total 'PIND <br /> 1,2-Dichloropropane ND Comments:i <br /> 1,3-Dichloropropane ND Surrogate Recoveries(`1o) <br /> 2,2 Dichloropropane ND Dibromoiluorontethane 96 <br /> 1,1-Dichloropropene ND Toiuene-d8 94 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 87 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in M"wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 05 ug/L;solid and sludge samples 5 ug/kg;Nvipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) 12-chloroethoxy) ethene; (d) 2-hexanorm (e) dichloromethane; (i) 2-butanone; {g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 li1 Edward Hamilton, Lab Director <br />