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Lancaster <br /> Laboratories .analysis Report <br /> 425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax:717-65&-2681•www.laneasteriabs.com <br /> Pagel of 4 <br /> Quality Control Summary <br /> Client Name: ChevronTexaco Group Number: 871649 <br /> Reported: 11/04/03 at 09:36 AM <br /> Laboratory Compliance Quality Control, <br /> Blank Blank Report LCS LCSD LC8/LCSD <br /> Analysis Name Result MDL Units %REC IRE C Limits RPD RPD Max <br /> Batch number: 032950013A Sample number(s) : 4147947-4147948 <br /> TPH - DRO CA LUFT (Waters) N.D. 50. ug/1 96 100 61-126 4 20 <br /> Batch number: 032950015A Sample number(s) : 4147947-4147952 <br /> Total TPH N.D. 40. ug/l 78 85 61-129 9 20 <br /> TPH Motor Oil C16-C36 N.D. 40. ug/l <br /> Batch number: 03295A16A Sample number(s) : 4147946-4147952 <br /> TPH-GRO - Waters N.D. 50. ug/l 112 100 70-130 12 30 <br /> Batch number: 032960024A Sample number(s) : 4147947-4147952 <br /> Methanol (by Direct Injection) N.D. 1000. ug/l 96 78-134 <br /> Batch number: 033030013A Sample number(s) : 4147949-4147952 <br /> TPH - DRO CA LUFT (Waters) N.D. 50. ug/l 76 70 61-126 9 20 <br /> Batch number: P032971AA Sample number(s) : 4147947-4147949 <br /> Ethanol N.D. 500. ug/l 95 46-145 <br /> Methyl Tertiary Butyl Ether N.D. 2. ug/l 103 77-127 <br /> di-Isopropyl ether N.D. 2. ug/1 104 74-125 <br /> thyl t-butyl ether N.D. 2. ug/l 98 74-120 <br /> Amyl methyl ether N.D. 2. ug/l 101 79-113 <br /> -Butyl alcohol N.D. 100. ug/l 99 53-147 <br /> Benzene N.D. .5 ug/1 103 85-117 <br /> 1,2-Dichloroethane N.D. 2. ug/1 102 77-132 <br /> Toluene N.D. .5 ug/l 94 85-115 <br /> 1,2-Dibromoethane N.D. 2. ug/l 93 81-114 <br /> Ethylbenzene N.D. .5 ug/l 94 82-119 <br /> Xylene (Total) N.D. .5 ug/l 95 84-120 <br /> Batch number: P032972AA Sample number(s) : 4147946 <br /> Methyl Tertiary Butyl Ether N.D. 2. ug/l 96 77-127 <br /> Benzene N.D. .5 ug/1 99 85-117 <br /> Toluene N.D. .5 ug/l 201 85-115 <br /> Ethylbenzene N.D. .5 ug/l 99 82-119 <br /> Xylene (Total) N.D. .5 ug/l 101 84-120 <br /> Batch number: P032981AA Sample number(s) : 4147950-4147952 <br /> Ethanol N.D. 500. ug/1 86 46-145 <br /> Methyl Tertiary Butyl Ether N.D. 2. ug/l 94 77-327 <br /> di-Isopropyl ether N.D. 2. ug/l 95 74-125 <br /> Ethyl t-butyl ether N.D. 2. ug/1 90 74-120 <br /> t-Amyl methyl ether N.D. 2. ug/l 95 79-113 <br /> t-Butyl alcohol N.D. 100. ug/l 99 53-147 <br /> Benzene N.D. .5 ug/l 95 85-117 <br /> 1,2-Dichloroethane N.D. 2. ug/l 94 77-132 <br /> Toluene N.D. .5 ug/1 94 85-115 <br /> 1,2-Dibromoethane N.D. 2. ug/1 94 81-114 <br /> Ethylbenzene N.D. .5 ug/l 96 82-119 <br /> Xylene (Total) N.D. .5 ug/l 95 84-120 <br /> Sample Matrix Quality Control <br /> *-Outside of specification <br /> 01) The result for one or both determinations was less than five times the LOQ. <br /> 2) The background result was more than four times the spike added. <br />