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Lancaster <br /> Laboratories Analysis Report <br /> d... <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 fax:717-656-2681•www.lanCaSterlabs.com <br /> Page 2 of 4 <br /> Quality Control Summary <br /> Client Name: ChevronTexaco Group Number: 871649 <br /> Reported-I1/04-/03at 0SI 3.6—AM <br /> Ms MSD MS/MSD RPD BKG DUP DUP DUP <br /> RPD <br /> Analyein Name %REC REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 03295A16A Sample number(s) : 4147946-4147952 <br /> TPH-GRO - Waters 111 63-154 <br /> Batch number: 032960024A Sample number(s) : 4147947-4147952 <br /> Methanol (by Direct Injection) 100 96 73-117 4 20 <br /> batch number: P032971AA Sample niimber(s)': 4147947-4147949 <br /> Ethanol 93 103 38-149 10 30 <br /> Methyl Tertiary Butyl Ether 103 103 69-134 0 30 <br /> di-Isopropyl ether 108 108 75-130 0 30 <br /> Ethyl t-butyl ether 100 101 76-119 1 30 <br /> t-Amyl methyl ether 103 104 77-117 1 30 <br /> t-Butyl alcohol 98 119 44-150 19 30 <br /> Benzene 110 109 83-128 1 30 <br /> 1,2-Dichloroethane 102 103 73-136 1 30 <br /> Toluene 101 101 83-127 1 30 <br /> 1,2-Dibromoethane 92 93 78-120 1 30 <br /> Ethylbenzene 101 103 82-129 2 30 <br /> Xylene (Total) 101 102 82-130 1 30 <br /> Batch number: P032972AA Sample number(s) : 4147946 <br /> Methyl Tertiary Butyl Ether 105 105 69-134 0 30 <br /> Benzene 109 110 83-128 0 30 • <br /> Toluene 113 114 83-127 1 30 <br /> Ethylbenzene 113 113 82-129 0 30 <br /> Xylene (Total) 114 113 82-130 1 30 <br /> Batch number: P032981AA Sample number(s) : 4147950-4147952 <br /> Ethanol 82 90 38-149 9 30 <br /> Methyl Tertiary Butyl Ether_ _ 97 95 69-134 2 30 <br />�di=lsopropyl ether 98 96 75=130 2 30 <br /> Ethyl t-butyl ether 92 92 78-119 1 30 <br /> t-Amyl methyl ether 97 95 77-117 2 30 <br /> t-Butyl alcohol 86 93 44-150 8 30 <br /> Benzene 103 100 83-128 3 30 <br /> 1,2-Dichloroethane 97 94 73-136 3 30 <br /> Toluene 103 102 83-127 1 30 <br /> 1,2-Dibromoethane 96 94 78-120 2 30 <br /> Ethylbenzene 104 103 82-129 1 30 <br /> Xylene (Total) 103 103 82-130 1 30 <br /> Surrogate Quality Control <br /> Analysis Name: TPH - DRO CA LUFT (Waters) <br /> Batch number: 032950013A <br /> Orthoterphenyl <br /> 4147947 99 <br /> 4147948 87 <br /> Blank 92 <br /> LCS 96 <br /> LCSD 97 <br /> Limits: 59-139 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> (2) The background result was more than four times the spike added. <br />