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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client. Equiva Services Service Request K9904880 <br /> Protect Inudent# 88870583/SAP#121258 Date Collected 6/29199 <br /> Sample Matrix Soil Date Received 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted NA <br /> Date Analyzed 7/29199 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Volatile Organic Compounds <br /> Sample Name SP-18AB COMP Units mg/L(ppm) <br /> Lab Code K9904890-054 Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Benzene EPA 1311 82606 02 1 0 5 ND <br /> Carbon TetraLhlonde EPA 1311 8260B 02 1 0 5 ND <br /> Chlorobenzene EPA 1311 8260B 02 1 100 ND <br /> Chloroform EPA 1311 8260B 02 1 6 ND <br /> 1,4-Dichlorobenzene EPA 1311 8260B 02 1 75 ND <br />. 1,2-Dichloroethane(EDC) EPA 1311 82602 02 1 05 ND <br /> 1,1-Dichloroethene EPA 1311 8260E 02 1 07 ND <br /> 2-Butanone(WK) EPA 1311 8260B 10 1 200 ND <br /> Tetraehloroethene(PCE) EPA 1311 8260B 02 1 0 7 ND <br /> Trichloroethene(TCE) EPA 1311 8260B 02 1 0 5 ND <br /> Vinyl Chloride EPA 1311 8260B 02 1 0 2 ND <br /> " From 40 CFR Part261,eta[ and Federal Register,March 29,1990 and June 29,1990 <br /> Approved By Date if-7 <br /> TCLPI522/052595 <br /> Page 36 <br />