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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Anahyticai Report <br /> Client Equiva Services Service Request K9904880� <br /> Project lnLident# 88870583/SAP#121258 Date Collected NA <br /> Sample Matrix Soil Date Received NA <br /> Date TCLP Performed. 7127199 <br /> Date Extracted: NA <br /> Date Analyzed 7129199 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Volatile Organic Compounds <br /> Sample Name Method Blank Units mg/L(ppm) <br /> Lab Code K990727-MB Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Benzene EPA 1311 8260B 0 2 1 0 5 ND <br /> Carbon Tetrachloride EPA 1311 8260B 0 2 1 0 5 ND <br /> Chlorobenzene EPA 1311 8260B 0 2 1 100 ND <br /> Chloroform EPA 1311 8260E 0 2 1 6 ND <br /> 1,4-Dichlorobenzene EPA 1311 8260B 0 2 1 7 5 ND <br /> 1,2-Dichloroethane(EDC) EPA 1311 8260B 0 2 1 05 ND <br /> 1,1-D►chloroethene EPA 1311 8260B 0 2 1 0 7 ND • <br /> 2-Butanone(MEK) EPA 1311 8260B 10 1 200 ND <br /> Tetrachloroethene(PCE) EPA 1311 8260B 0 2 1 0 7 ND <br /> Tnchloroethene(TCE) EPA 1311 8260B 0 2 1 05 ND <br /> Vinyl Chlonde EPA 1311 8260B 0 2 1 0 2 ND <br /> * From 40 CFR Part 261,0 al,and Federal Register,March 29, 1990 and June 29, 1990 <br /> Approved By Date �f �S •+ <br /> TCLPIS221052595 <br /> Page 37 <br />