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05/19/2003 08:25 2094671118 AGE STOCKTON PAGE 07 <br />Mas 14 2003 11:08AM CRMPBELL ANALYTICAL i- 3-799—IG20 p.7 <br />110 2114 Avenue Soath, M07, Pacheco, CA 94539-5560 <br />McCampbell Analytical Inc. Telophont ; 925-799-1620 xag : 92s -79e-16;7 <br />LAA <br />Advanced C3eoPhvironn=tel, Inc. Client Project ID: Flag City Chevron 1 Date Sampled: 05/07/03 <br />837 Shaw Road Date R.cccivod: 05/08/03 <br />Stockton, GA 95215 Client Contact. Tim Cuellar Date Extract -,d; 05(08/03 <br />Client P.O,; Date Analyzed; 05/09/03-05/10/03 <br />Oxygenated Volatile Organics by 1('&T and GC/MS* <br />EX0669M Method: 9W 50.%m Anab-tical Madz4. 5W 82608 work Order. 0305124 <br />Lab ID <br />(M5124 -MIA <br />0305124-002A ! 0305124-003A 0305124-004A <br />Reporting Limit for <br />OF x] <br />Client ID <br />DSP -1 <br />DSP -2 DSP -3 DSP -4 <br />Matrix <br />S <br />....---�... <br />1 <br />ND <br />S S S <br />_._._ _-.__._...: --.-. - - ...... <br />4 1 10 <br />Concentration <br />ND<20 ND ND<0 <br />DF <br />Compound <br />Diisopropylether (DIMB) <br />S <br />µg/Kg <br />5,0 <br />W <br />uglL <br />NA <br />Sth)t tert-butyl cher (ETRE) <br />ND <br />NDQO <br />ND <br />NO <br />ND<S0 <br />NDa50 <br />S-0 <br />NA <br />Habyl-t-butylether (MTB£) <br />ND <br />l$0 <br />5.0 <br />3.0 <br />NA <br />NA <br />text amyl methyl ether (TAME) <br />ND <br />ND<«0 <br />ND NIK50 <br />t -Butyl alcobol (TBA) <br />Nb <br />130 <br />NI) <br />NIICLI p <br />25 <br />NA <br />Surrogate Recoveries <br />%SS: 113 109 112 96,7 <br />Cotttmenta <br />'vAW and vapor aamplea and all TCLP & SPLP c7araCta are repor Od in 1191L, 50illeludgaisolid samples in µspoil, wipe t:amplcg ib pghalpe, <br />product-loil/non aqueous liquid sdmplea in mg/L. <br />ND mems riot de=ted ailovethe reporting limit; N/A means analyte not applicable to this analysis, <br />h) lighter than water immiscible ebeeniproduct is present; i) liquid sample that contains greater than —2 vol. % sediment; j) sample diluted due to high <br />3rgenic c°nteni. <br />DHS Ceniflcation No. 1644 <br />Angela Rydelius, Lab Manager <br />I 9 9 1 <br />