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05/19/2003 08:25 2094671118 AGE STOCKTON PAGE 08 <br />Mai 14 2003 lI:C9AM ;CAMPBELL ANALYTICAL 1 .5-798-1620 P.8 <br />Analytical <br />110 2nd Avartue south #D7,, I wAecp, ca. 84553-5560 <br />�CCa127t1beU }C, <br />i'Telephone <br />: 9z5-798-I62o Fax :923-79B-1Gi7 <br />http.'1aww.mccat*49.o0m E UJI <br />hW9ggLb@Il-oam <br />Advanced Geolimvironmcrlta[, Inc. <br />Client Project ID: Flag City C lnovron <br />Date Sample d: <br />05/07/03 <br />837 Shaw Road <br />Date Receivtod: <br />05108/03 <br />Stockton, CA 95z15 <br />Client Contact: Tim Cuellar <br />Date E.xtxact,g)d- <br />05/08/03 <br />Client P,O.; <br />bate Analyzed; <br />05/09/03-05/10/03 <br />Oxygenated Volatile Orgtmics by P&T and GC/M9^ <br />Exhget=Method,. SW5030B Analytical Meth04_SW826OEt <br />work Ozder.0305124 <br />Lab ID <br />0305124-005A <br />0305124.006A 0305124-007A 0305124-OOSA <br />Client ID <br />DSP -5 <br />D5P-6 <br />PL -1 <br />pl .2 <br />Reporting Limit for <br />Matrix <br />S <br />g� � S � 8 <br />AP �l <br />DP <br />......_._.. <br />---... <br />1 <br />_..,_._.. �.......... ...__._, <br />1 1 <br />1 <br />s <br />W <br />Compound <br />Concentration <br />u�>3 <br />ug'L <br />Diisopropyl ether (DipE) <br />NO <br />ND <br />ND <br />NOD <br />5.0 <br />NA <br />Ethyl ten -butyl cher (ET13S) <br />ND <br />ND <br />ND <br />NJD <br />5.0 <br />NA <br />Metbyk-butyl eth- (MTBE) <br />3 5 <br />42 <br />11 <br />ND <br />3.0 <br />NA <br />tart-Awy,I methyl ether (TAME) <br />ND <br />ND <br />ND <br />ND <br />5.0 <br />NA <br />t -Butyl alcohol (TBA) <br />31 <br />ND -T <br />56 <br />Nn <br />25 <br />NA <br />Surrogate Reooveries <br />%SS: <br />98.1 <br />94.0 <br />97,1 <br />99.4 <br />Cort�entx <br />,,.r_, <br />" water and vapor sampleF and all TCU & SPLP extracts are ncportod in µglL, soWsludge/solid samples in <br />gg/kg, wipe t arttplee <br />in <br />nnduetloil/non-aqueous liquid samples in mg/L. <br />µg/wipe, <br />VD means not detected above the reporting limit; N/A means analyte not applicable to this analysis. <br />t) tighter than water immiacihle sheetVproduct is present; i) liquid sample that eontaina greater than --2 vol, % sediment; <br />w'ganic oontcnt. i) sample <br />diluted due to high <br />DHS CortificatioiaNv, 1644 <br />Angela Rydebus, Lab Manager <br />