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05/19/2003 08:25 2094671118 AGE STOCKTON PAGE 09 <br />May 14 2003 11:05RM ;CAMPBELL. ANFiLYTICAL 1 .5-799-1620 p-9 <br />110 2nd Avenue Sovtb, #D7, Pacheco CA 94553-556o <br />McCampbell AnEdytical Inc. TeIapbone!925-798-1620 Pax:925.799-1627 <br />:i/www,moo bell-caan P.nnit; main bell.eom <br />Advanced GeoFavixonnvzAal, Inc. Client Project ID: Flag City Chevron Date Sampled; 05/07/03 <br />837 Shaw Road Date Receivod. 05/08/03 <br />Stockton, CA 95215 Client Contact Tim CueU,ar Date Extract;!d: 05/08/03 <br />Surrogate Recoveries (%) <br />e%5S: 98,2 96.7 98.1 95.6 <br />Comments <br />watear and vapor satnoc;3 and all TC1 P & SPLP extracts are reported in g9tL, wil/sludgo/solid Samples in ASIC , wipe sartlples in uP/x ipe, <br />ar0ductloil/non-aquct us liqusa <br />id mples in mga- <br />ND menus not detected abovethc repotting limit; N/A means analyte riot appEcable to this analysis. <br />i) li$htcr than water itmnincihle sheen/product is present; i) liquid sample that contains greater than -2 vol. N sediment; i) eam.ple diluted due to high <br />)rganic content. <br />DHS CerWication Na. 1644 <br />la Rydeliiug, Lab bdauager <br />Client P.U: <br />Date AMI)w,d; 05109/03-05/10103 <br />Oxygenated <br />Volatile <br />Organics by P&T and GC/MS* <br />ExtraHmMahod: Sw50309 <br />Ana>y1IcuA4ethod:SWB2b0a <br />WvrkOtcbr:0305124 <br />Lab ID <br />0305124-009A <br />0305124.-010A � <br />�— <br />PL -4 <br />0305124IA 0305124-012A <br />YL -5^ <br />pL-5 <br />Client ID <br />pL-3 <br />Repotting Limit far <br />Matrix <br />S <br />S <br />S <br />S <br />DF =1 <br />DF <br />Compound <br />Concentration <br />yrg/ICg ugh[, <br />Diisopropyl ether (DFF) <br />ND <br />ND7ND <br />ND <br />5,0 NA <br />Bthyl tett-butyl etbcr ();TBE) <br />1� <br />ND <br />� <br />NA <br />15 <br />5.0 NA <br />Meryl -t -butyl shier (MTBE) <br />2g <br />ND <br />12 - <br />ND <br />5.0 NA <br />5-0 NA <br />Cert -Amyl trraftl ether (TAME) <br />ND <br />t-Bu:yi alcohol (TBA) <br />30 <br />ND — <br />NA <br />25 NA <br />Surrogate Recoveries (%) <br />e%5S: 98,2 96.7 98.1 95.6 <br />Comments <br />watear and vapor satnoc;3 and all TC1 P & SPLP extracts are reported in g9tL, wil/sludgo/solid Samples in ASIC , wipe sartlples in uP/x ipe, <br />ar0ductloil/non-aquct us liqusa <br />id mples in mga- <br />ND menus not detected abovethc repotting limit; N/A means analyte riot appEcable to this analysis. <br />i) li$htcr than water itmnincihle sheen/product is present; i) liquid sample that contains greater than -2 vol. N sediment; i) eam.ple diluted due to high <br />)rganic content. <br />DHS CerWication Na. 1644 <br />la Rydeliiug, Lab bdauager <br />