Laserfiche WebLink
11/07/2002 1.1:32 2C946�'" ; -3 FIFTH FLOOR PAGE 0 <br />MINIMUM VERIFICATION LAB(3RATORYANALYSIS <br />TANK <br /># <br />TANK <br />CO;hTTENTS <br />TPH-G <br />8015 <br />$260 <br />TPH-1) <br />(1015 <br />$260 <br />pyX &B <br />$020 <br />8260 <br />CL <br />CL HC <br />� <br />$240 <br />8260 <br />TOTAL. <br />I.I;AD <br />7424 <br />7421 <br />IvITBE <br />8020 <br />8269 <br />OXYGEN t�s+rar <br />RTES' <br />(Mi'BL, ICRP! <br />TSA,DtPE, AES or <br />$TBE. <br />TAME) AA <br />PCM <br />8270 <br />8080 <br />626D <br />LEADED GAS <br />X <br />x <br />x <br />X <br />T7NL GAS <br />.X <br />x <br />X <br />DIESEL. <br />x <br />x <br />KERDSENE <br />X <br />i x <br />X <br />UNK FUEL. <br />X <br />X <br />I X <br />X <br />X <br />PROD. OIL <br />X <br />I x <br />x <br />CHLOR <br />SOLVENTS <br />I <br />I X <br />.X <br />X. <br />NONCHLOR <br />SOLVENTS <br />x <br />X <br />X <br />WASTED <br />USED OILX <br />X' <br />X <br />1 <br />X <br />X <br />X <br />X <br />All nnnlv,;,t <br />_T <br />_+), ;� o .k.. 1_ <br />_. t rn <br />_" <br />a ,.. <br />____ __ —_ _-5____ ui .-, uu wv • urbw1vau in LCA Z)vv 640. 1=0 rditzon, Those tmthods not found in SW 846 alt <br />specifically noted below. Refer to rhe "SWRC13 LOFT Field Manuel", Appendix D (B), Table 3-5 on page A20 for minim m d.etectior <br />limits for rmlor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendetions for Initial Evaluation anc <br />Investigation of UST's" for, the waste and motor oil minimum detection limits. Detection Limits that remain below the MCL, STYC oy <br />Allowable Limit of the contaminant in question will be accepted, however laboratory shall utilize the most conservative method. <br />LABORATORY ANALYSES TERMINOLOGY: <br />TP!T-G Total Perrolcum hydrocarbon, Gasoline, GVFID (5030) 8015 mod or GCIMS 8260 <br />TPt H -D Total Petroleum Hydrocarbon, Diesel, GUFID (3550), 8015 mod or GC/MS 8260 <br />BTX & ERcnzene, Toluene, Xylcnc & Ethyl Benzene, GC/PM 8020 or GC'NIS 8260 <br />CL HC Chlorinated Hydrocarbon, GCIHSD 8010, GC/MS 540 or 8260 <br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP -AES 6010 <br />OXYGENATES MTBE, ETRE, TAME, RIPE, & TBA CS 8260 (For MTBE. Screen only you may use 8020) <br />METALS ICRP or AA Inductively Ceuplcd Plasm Atointc !✓mission Spectrometry 6010 or Atomic ,absorption Spectrotnetry 7'000. Metals: <br />Cirdnziu r4 Chromium III acid VI, Lead, Zinc and Nickel. <br />PCa Polychlorinated Biphenyls, C•CIMS 8270 or 8080 <br />CC -FID Gas ChrorratOgraphy, Flame Ionization Dcicction <br />Method 3050 Acid digestion <br />Method 3540 Soxhlet sample preparation <br />Method 3550 Sonication sarnplc preparation, extraction I thod <br />M.-thod 5030 FWVC and trap sample prepsratinn <br />QA/QC Quality Assurance/Quality Control <br />Notts. To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns ate preferred to packed columns; a <br />packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons have been charaetGrizcd aid proper QA/QC is followed. For <br />drinking water sources, EPA recommends tbat the 500 series for volatile organic should be used in preference to the 600 series because the detection <br />limits are lower And the QA/QC is better. Sarrtpics cxht'blting airy level of heavy metal exntarnivation may require farther analysis. KTS AHD <br />recon mbttds holding those samples until disposal is indit^.atcd. <br />i <br />EH 23 046 (Revised 05/09/00) <br />