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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' htt //www mccam bell corn E-mail train@mccampbell corn <br /> • <br /> ' Date Sampled 03/21/01 <br /> Advanced GeoEnvironmentai Client Project ID Chase Madison <br /> Date Received 03/23/01 <br /> 837 Shaw Road <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03/23/01 <br /> Client P O Date Analyzed 03/23-03126101 <br /> i <br /> CAM 1 CCR 17 Metals* <br /> [H-PA methods 6010/200 7 7470174711245 11245 5(Hg) 7060/206 2(As) 77401270 2(Se) 7841/279 2(Tl) 239 2(Pb,water matrix) <br /> Lab ID 63690 <br /> Reporting Limit <br /> Client 1D SSW-9' <br /> Matrix S S W STLC <br /> ' TCLP <br /> Extracttan° TTLC TTLC TTLC <br /> Compound Concentration' mg/kg mglL mg/L <br /> Antimony(Sb) 5 1 2 5 0 006 005 <br /> Arsenic(As) ND 2 5 0 005 025 <br /> ' Barium(Ba) 190 25 005 005 <br /> Beryllium(Be) 053 05 0 004 001 <br /> ' Cadmium(Cd) ND 05 0 005 001 <br /> Chromium(Cr) 51 05 002 005 <br /> Cobalt(Co) 15 20 005 005 <br /> Copper(Cu) 33 20 005 005 <br /> Lead(Pb) l 8 30 0 005 02 <br /> ' Mercury(Hg) ND 006 0 0008 0 005 <br /> Molybdenum(Mo) ND 20 0 05 005 <br /> Nickel(Ni) 38 20 0 Os 005 <br /> Selenium(Se) ND 25 0 005 025 <br /> ' Silvei (Ag) ND 1 0 001 005 <br /> Thallium(Tl) ND 25 0 005 05 <br /> Vanadium(V) 60 20 005 005 <br /> ' Zinc(Zn) 65 1 0 005 0 05 <br /> %Recovery Surrogate 105 <br /> Comments �A <br /> R water samples aie reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> EPA eruacnort methods 131 1(TCLP),3010/3020(water,TTLC),3040(orgami,matrices,TTLC),3050(solids,TTLC) STLC-CA Title 22 <br /> w DISTLC extractions are performed using STLC methodology except that deionized water is substituted fol citric acid buffer as the <br /> . extraction iluld DISTLC results are not applicable to STLC regulatory limits <br /> "sun ogate dsluted out of range <br /> ' reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than --2 vol % sediment this sediments extracted with the liquid, in accordance with EPA <br /> methodologies and c.an significantly effect reported metal concentrations <br /> ' DHS Certification No 1644 2__Edward Hamilton, Lab Director <br />