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1 <br /> I W 2nd Avenue South #D7, Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http llwtivw mccarnpbell com E-mail main@mc(,ampbell Lom <br /> ' Advanced GeoEnvrronmental Client Project ID Chase Madison Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/23/01 <br /> ' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03/23/01 <br /> Client P O Date Analyzed 03/23-03/26/01 <br /> CAM/CCR 17 Metals* <br /> EPA methods 6010/200 7 747017471/245 1/245 5(lig),7060/206 2(As) 7740/270 2(Se),7841/279 2(Tl),239 2(Pb water matrix) <br /> Lab ID 63682 63683 63684 _ 63685 <br /> RLpoinnu Limit <br /> Client 11) SSW-5' SSN-5' TKN-5' TKF-9' <br /> Matrix S S S S S W STLC, <br /> TCLP <br /> .Extraction° TTLC TTLC TTLC TTLC TTLC ['TLC <br /> Compound Concentration* mg/kg mg/L mg/L <br /> Antimony(Sb) ND 99 ND 13 25 0 006 005 <br /> Arsenic(As) ND ND ND ND 25 0 005 025 <br /> Barium(Ba) 270 200 120 150 2S 005 005 <br /> Beryllium(Be) 070 057 ND ND 05 0 004 001 <br /> Cadmium(Cd) ND ND ND 051 05 0 005 001 <br /> ' Chromium(Cr) 59 59 40 39 05 002 005 <br /> Cobalt(Co) 18 22 13 10 20 005 005 <br /> Copper(Cu) 45 40 31 26 20 005 005 <br /> Lead(Pb) 18 17 12 10 3 0 0 005 02 <br /> Mercury(Hg) 0 074 ND ND ND 006 00008 0 005 <br /> Molvbdenum(Mo) ND ND ND ND 20 0 OS 005 <br /> Nickel(Ni) 48 50 36 32 20 005 0 05 <br /> Selenium(Se) ND ND ND ND 25 0 005 0 25 <br /> Siler(Ag) ND ND ND ND 1 0 0 01 005 <br /> ' Thallium(Tl) ND ND ND ND 25 0 005 05 <br /> Vanadium(V) 75 62 39 36 20 005 005 <br /> ' Zinc(Zn) 69 71 52 55 1 0 005 00- <br /> % <br /> 05%Recovery Surrogate 104 98 101 l01 <br /> Comments <br /> * water samples are reported in mg/L,soil and sludge,samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> °CPA extraction methods 131/(TCLP),3010/3020(water f TLC) 3040(arganiL matrices,TTLC) 3050(solids,TTLC) STLC CA Title 22 <br /> " DISTLC ertraLtions are performed using STLC methodology except that deionized watei is substituted for citric acid butter as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> " <br /> surrogate diluted out of range <br /> ' &ieportmg limit raised due to matrix interference <br /> i) liquid sample, that contains greater than --2 vol % sediment this sediment is extracted with the liquid in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> ' DHS Certification No 1644 Edward Hamilton, Lab Director <br />