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110 2nd Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCA1MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http//vrwAvmccampbellcorn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project M Chase Madison Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/23/01 <br /> ' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03!23101 <br /> Client P O Date Analyzed 03/23-03126101 <br /> ' CAM 1 CCR 17 Metals* <br /> EPA methods 6010/200 7,7470/7471/245 1/245 5(Hg),7060/206 2(As),7740/270 2(Sc) 7841/279 2(Tl) 239 2(Pb,water matrix) <br /> Lab ID 63686 63687 63688 63689 <br /> Reporting Limit <br /> ' Client ID TKW-5' TKE-5' TKS-5' SSN-9' <br /> Matrix S S S S S W STLC <br /> Extraction° TTLC TTLC TTLC LC TTLC TTLC TCI-P <br /> TT <br /> _ J <br /> Compound Concentration* mg/kg mg/L mg/L <br /> Antimony(Sb) 5 3 ND 47 47 25 0 006 005 <br /> Arsenic(As) 2 8 3 3 ND ND 25 0 005 025 <br /> Barium(Ba) 290 270 190 120 25 005 005 <br /> Beryllium (Be) 062 083 0 G9 ND 05 0 004 0 0 t <br /> Cadmium(Cd) 053 ND ND ND 05 0 005 1 001 <br /> ' Chromium(Cr) 62 73 58 1 40 05 002 005 <br /> Cobalt(Co) 17 17 21 11 20 005 005 <br /> ' Copper(Cu) 39 49 44 25 20 005 005 <br /> Lead(Pb) is 18 17 12 30 0 005 02 <br /> Meicury(Hg) ND ND ND ND 006 00008 0 005 <br /> Molybdenum(Mo) ND ND ND ND 20 005 0 05 <br /> ' Nickel(Ni) 49 56 50 30 20 005 005 <br /> Selenium(Se) ND ND ND ND 25 0 005 025 <br /> Sliver(Ag) ND ND ND ND l 0 001 005 <br /> Thallium(Tl) ND ND ND ND 25 0 005 05 <br /> Vanadium(V) 60 88 69 45 20 005 005 <br /> ' Zinc(Ln) 64 82 72 47 1 0 005 005 <br /> %Recovery Surrogate 101 100 99 102 <br /> Comments <br /> *water samples aie reported in irg/L,soil and sludge Samples in mg/kg,wipes in tig/wipe and all TCLP/STLC/SPLP extracts m mg/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> °EPA cxtrauiori methods 1311(TCLP),3410/3020(water,T1LC),3040(organrc matnces,TTLC),3050(solids,TfLC) STLC-CA Title 22 <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the <br /> . extraction fluid DISTLC results are not applicable to STLC iegulatmy limits <br /> "surrogate diluted out of range <br /> ' iepoi ting limit raised due to matrix interference <br /> i) liquid sample that contains greater than —2 vol % sediment this sediment extracted with the liquid, in accoidance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />