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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAN2BELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htto//www mccMpbell com E-mail main@,mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Chase./Madison Date Sampled 02/13/2002 <br /> 837 Shaw Road Date Received 02/15/2002 <br /> ' Stockton, CA 95215 Client Contact Paul Dotson. Date Extracted.02/15-02/21/2002 <br /> Client P O Date Analyzed 02/15-02/2112002 <br /> Gasoline Range(C6-CT2) Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether*&BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602 Uifomia RWQCB(SF Bay Region)method GCF1D(5030) <br /> Lab IDClient ID Matrix TPH(g)* MTBE Benzene Toluene Ethyl Xylenes %Recovery <br /> benzene Surrogate <br /> 90455 MW10022 -13- W ND ND ND ND ND ND 101 <br /> 1 90456 MW/02-13- W ND ND ND ND ND ND 100 <br /> 02 <br /> 90457 MW4022 -13 W ND ND ND ND ND ND 109 <br /> ' 90458 MW13/02- W ND ND ND ND ND ND 108 <br /> 13-02 <br /> 90459 MW19A/02- W ND ND ND ND ND ND 105 <br /> ' 13-02 <br /> 90460 MW19B/02- W ND ND ND ND ND ND 104 <br /> 13-02 <br /> , . 90461 MW20A/02- W ND ND ND ND ND ND 114 <br /> 13-02 <br /> 90462 MW20B/02- W ND ND ND ND ND ND 105 <br /> 13-02 <br /> ' 90463 N1W31 02- W 4500,e,a ND 360 27 200 12 ---4 <br /> -02 <br /> 90464 lVfW310B/02- W 700,e ND<20 ND 30 <br /> Reporting Limit unless W 50 ug/L 50 05 05 05 05 <br /> otherwise stated ND <br /> means not detected above' <br /> the reporting limit S 10 mg/kg 005 0 005 0 005 0 005 0 005 <br /> "water and vapor samples are reported in ug/C.,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> "cluttered chromatogram,sample peals coeiutes with surrogate peak <br /> 'The following descriptions of the TPH chromatogram are cursory m nature and McCampbelI Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are signiffcarit(aged <br /> ' gasoltne9), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant, biologically altered gasolrnO, e) TPH pattern that does not appear to be derived from gasoline <br /> (stoddard solvent?) f)one to a Yew isolated peaks present, g)strongly aged gasoline or diesel range compounds are sigficant,h)lighter <br /> than water inirmscible sheen is present,i)Iiquid sample that contains greater than—5 vol %sediment,j)no recognizable nauern <br /> ' DHS Certification No 1644 Edward Hamilton,Lab Director <br />