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II <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' McCAMPSELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-I622 <br /> http.//www mccampbell com E-mail mam@rnecampbell com <br /> Advanced GeoEnvironmental Client Protect ID Chase/Madtson Date Sampled 02/13/2002 <br /> 837 Shaw Road Date Received 02/15/2002 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 02/15/2002 <br /> ' Client P O Date Analyzed 02/15/2002 <br /> Diesel Range(C10-C23) and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510,California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Laic M Client ID Matrix TPH(d)- TPH(mo)+ %Recovery <br /> S urrogate <br /> 90455 MW 1102-13-02 W ND ND 101 <br /> 90456 MW2/02-13-02 W ND ND 102 <br /> 90457 MW4/02-13-02 W ND ND 101 <br /> 90458 MW13/02-13-02 W ND I ND 102 <br /> 90459 MW19 X02-13- W ND ND 101 <br /> 90460 MW19B/02-13- W ND NU 100 <br /> 1 90461 MW20�02-13- W 190,c,f ND 101 <br /> 90462 MW20B/02-13- W ND ND 99 <br /> 90463 MW21A/02-13- W 7700,d,b 930 101 <br /> 90464 MW21B/02-13- W 620,d,b ND 103 <br /> 02 <br /> Reporting Limit unless otherwise W 50 ug/L 250 ug/L <br /> ' stated,ND means not detected above <br /> the reporting limit S 1 0 mg/kg 5 0 mg/kg <br /> *water samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STLC/SPLP extracts in <br /> ' ug(1. <br /> A cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrogate has been <br /> drnunished by dilution of original extract <br /> ' '17ie following descriptions of the TPH chromatogram are cursory in nature and McCarnpbell Analytical is not responsible for their <br /> interpretation a)unmodified or weakly modified diesel is significant,b)diesel range compounds are significant no recognizable pattern,c) <br /> aged diesel? is significant),d)gasoline range compounds are significant,e)medium boiling point pattern that does not match diesel (?), f) <br /> ' one to a few isolated peaks present, g)oil range compounds are significant, h) lighter than water imrmscible sheen is present, i) liquid <br /> sample that contains greater than—5 vol %sediment <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />