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[u <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbellco E-mail train@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Gewcke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Bnan Millman Date Extracted 03121-03127/2002 <br /> LChent P O Date Analyzed 03/21-03/27/2002 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab 1D 0203321- 0203321- 0203321- 0203321- <br /> 009 Ol 0 Oil 012 Reporting Limit <br /> Client ID MW8/03180 MW9/03180 MW10/0318 MW11/0318 <br /> 2 2 02 02 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND ND 50 1 0 <br /> Ethyl tert-Butyl Ether(FTSE) ND ND ND ND 50 10 <br /> . Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> tert-Butanol ND ND<10 ND ND 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 97 97 96 100 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,{1}sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />