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(vi <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell co m E-mail mam@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21-03/27/2002 <br /> Client P 4 Date Analyzed 03/21-03/27/2002 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 0203321- 0203321- 0203321- <br /> 013 014 015 <br /> MW12/0318 MW13/0318 MW14/0318 Reporting Limit <br /> Client ID 02 02 02 <br /> Matrix W W W s W <br /> Compound Concentration* ug/kg ug/L <br /> De-isopropyl Ether(DWE) ND ND ND<50 50 1 0 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND<50 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND<50 I'll <br /> 0 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<50 so 10 <br /> tert-Butanol ND ND ND<500 25 50 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 96 97 89 <br /> Comments <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />