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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> ht ://www.mccarnbell-com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br /> IStockton, CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client P.O: Date Analyzed: 03/16-03/20/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 . <br /> Lair ID 62944 <br /> Client ID E W 1/03-14-01 <br /> Matrix W <br /> Reporting Limit - Rcporting Limit <br /> Compound Concentration* W S Compound Concentration* F5.10 <br /> S <br /> Acetone ro) ND 5.0 25 trans-l,3-Dichloropropenc ND 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethaire ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Ile Carbon Tetrachloride ND 1 1.0 5.0 Methyl tert-Butyl Ether(MTBE) -- 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether" ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> I Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> I 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND. 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br />' I,1-Dichlornethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane 9.9 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethenc ND 1.0 5.0 Vinyl Acetate ° ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride " ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 1 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND i.0 5.0Dibromofluoromethane 109 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1.0 5.0() <br /> .0 4-Bromotluorobenzene 94 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> I chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />