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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone.925-798-1620 Fax .925-798-1622 <br /> htir://www.mcca!npbell.com E-mail:main@mccatnpbell.cotn <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton, CA 95215 Client Contact: Brian Millman Date Extracted: 03116-03/20/01 <br /> Client P.O: Date Analyzed: 03116-03/20/01 <br /> IVolatile Organics By GC/MS <br /> EPA method 8260 - <br /> Lab ID - 62945 <br /> Client ID MWI/03-14-01 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br /> W S w S <br /> Acetone(e) ND 5.0 25 0-ans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1-0 5.0 Etbylbenzene ND 1.0 5.0 <br /> I Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichlorotnethane ND 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND LO 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-lsopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride° ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 l0 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyi ketone'8' ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) --- 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Eth ° ND 1-0 5.0 Styrene ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoiuene ND 1.0 5.0 Toluene 11 ND 1.0 5.0 <br /> I Dibromochlommethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chlompropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> IJ-Dichloroethane ND 1-0 5.0 1,2,4-Trimethyibenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane 2.7 1.0 5.0 1,3,5-Trimethylbenzene 1.1 1.0 5.0 <br /> IJ-Dichloroethene ND 1.0 5.0 Vinyl Acetate ') ND 5.0 25 <br /> cis-1,2-Dichioroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> trans-12-Dichloroethene ND 1.0 5.0 Xylenes,total l.2 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 107 <br /> 1,I-Dichloropropene ND 1.0 5.0 Toluene-d8 92 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene L95 <br /> water and vapor samples are reported in ug/1-soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains,greater than -5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chlotoethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />