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I110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> http://ww-w.mEcl bell.com E-mail:main@mccampbell.com <br /> • <br /> IAdvanced GeoEnvironmental CIient Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton, CA 95215 Client Contact: Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client P.O: Date Analyzed: 03/16-03/20/01 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 62950 <br />' Client ID MW6/03-14-01 <br /> Matrix I W <br /> Reporting Limit Reporting Limit <br /> Compound Concentration* w S Compound Concentration* W S <br />' Acetone i ND 5.0 25 trans-l,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1,0 5.0 p-Isopropyi toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride(`) ND<2.0 1.0 5.0 <br /> tcrt-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketones ND 1.0 5.0 <br /> • Carbon Tetrachloride ND 1.0 5.0 Methyl tort-Butyl Ether(MTBE) --- 1.0 5.0 <br /> Chlorobenzene ND L0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether" ND 1.0 5.0 Styrene ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Triehlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzenc ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br />' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND ].0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> IJ-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride " ND 1.0 5.0 <br />' ttans-t,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropmpane ND i.0 5.0 Comments: <br /> 1,3-Dichloropmpane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropmpane ND 1.0 5.0 Dibromofluommethane 109 <br />' 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 96 <br /> cis-1,3-Dichloropmpene ND 1.0 5.0 4-Bromofluorobenzene 96 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chioroethoxy) ethene, (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> • pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than -5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; ) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />