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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br /> hgR://www.mccampbell.com E-mail:main@mccampbell.com <br /> i <br /> Advanced GeoEnvironrnental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br /> Stockton, CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03/20101 <br /> Client P.O: Date Analyzed: 03/16-03/20101 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62949 - <br /> Client ID MW5/03-14-01 <br /> Matrix W <br /> Compound Concentration* Rep°rihng Limit Compound Concentration* RqwtiRg Limit <br />' W S W S <br /> .Acetone ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichlorornethane ND LO 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND' 1.0 5.0 <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride(c) NDC2.0 1.0 5A <br /> tert-Butyl benzene ND I.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isohutyl ketone ND 1.0 5.0 <br />' Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether` ND 1.0 5.0 Styrene ND 1.0 5.0 - <br /> Chloroform <br /> AChloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br />' 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND LO 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND I.0 5.0 <br />' 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichlorocthane 10 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate °' ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride " ND 1.0 5.0 <br />' trans-1,2-Dichloroethene ND 1.0 5.0 Xylene5,total ND 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%} <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 108 <br />' 1,1-Dichloropropene ND 1.0 5.0 Toluene-dS 95 <br /> c1s-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 96 <br /> water and vapor samples are reported in ug/1„soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPI,P extracts in ug/L <br />' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanonc or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than -5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; ) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dirriethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />