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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMTBELL A.NA.LYTICA.L INC. Telephone: 925-7981620 Fax :925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke . Date Sampled:03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton, CA 95215 Client Contact:Brian Millinan Date Extracted: 03/16-03/20/01 <br />' Client P.O: Date Analyzed: 03/16-03/20101 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62953 <br />' Client ID MW9/03-14-01 <br /> Matrix W <br /> * Reporting Limn - * Reportag Limit <br /> Compound Concentration Compound Concentration <br />' W S W S <br /> Acetone ebi ND<15 5.0 25 trans-l,3-Dichloropropene ND<2.5 1.0 5.0 <br /> Benzene 3.0 1.0 5.0 Ethylene dibromide ND<2.5 1.0 5.0 <br /> Bromobenzene ND<2.5 1.0 5.0 Ethylbenzene 34 1.0 5.0 <br />' Bromochloromethane ND<2.5 1.0 5.0 Hexachlorobutadiene ND<13 5.0 25 <br /> Bromodichloromethane ND<2.5 1.0 5.0 lodomethane ND<2.5 1.0 5.0 <br /> Bromoform ND<2.5 1.0 5.0 Isopropyibenzene 7.1 1.0 5.0 <br /> Brumomethane ND<2.5 1.0 5.0 p-Isopropyl toluene 4.8 1.0 5.0 <br />' n-Butyl benzene ND<2.5 1.0 5.0 Methyl butyl ketone ND<2.5 1.0 5.0 <br /> sec-Butyl benzene ND<2.5 1.0 5.0 Methylcne Chloride(t) ND<5.0 1.0 5.0 <br /> tert-Butyl benzene ND<2.5 1.0 5.0 Methyl ethyl ketone` ND<5.0 2.0 10 <br /> Carbon Disulfide ND<2.5 1.0 5.0 Methyl isobutyl ketone`s ND<2.5 1.0 5.0 <br />' Carbon Tetrachloride ND<2.5 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND<2.5 1.0 5.0 Naphthalene 45 5.0 5.0 <br /> Chloroethane ND<2.5 1.0 5.0 n-Propyl benzene ND<2.5 1.0 5.0 <br />' 2-Chloroethyl Vinyl Ethe ND<.5 1.0 5.0 Styrene ND<2.5 1.0 5.0 <br /> Chloroform ND<2.5 1.0 5.0 1,1,1,2-Tetrachloroethane ND<2.5 1.0 5.0 <br /> Chloromethane ND<2.5 1.0 5.0 1,1,2,2-Tetrachloroethane ND<2.5 1.0 5.0 <br /> 2-Chlorotoluene ND<2.5 1.0 5.0 Tetrachloroethene ND<2.5 1.0 5.0 <br />' 4-Chlorotoluene ND<2.5 1.0 5.0 Toluene` ND<2.5 1.0 5.0 <br /> Dibromochlorometbane ND<2.5 1.0 5.0 1,2,3--Trichlorobenzene ND<13 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<5.0 2.0 10 1,2,4-Trichlorobenzene ND<13 5.0 25 <br /> DibrOMOmethane ND<2.5 1.0 5.0 1,1,1-Trichloroethane ND<2.5 1.0 5.0 <br />' 1,2-Dichlorobenzene ND<2.5 1.0 5.0 1,1,2-Trichloroethane ND<2,5 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<2.5 1.0 5.0 Trichloroethene ND<2.5 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<2.5 LO 5.0 Trichlorofluoromethane ND<2.5 1.0 5.0 <br /> Dichlorodifluoromerbane ND<2.5 1.0 5.0 1,2,3-Trichloropropane ND<2.5 1.0 5.0 <br />' ],l-Dichloroethane ND<2.5 1.0 5.0 1,2,4-Trimethylbenzene 220 1.0 5.0 <br /> 1,2-Dichloroethane 59 1.0 5.0 1,3,5-Trimethylbenzene 85 1.0 5.0 <br /> 1,1-Dichloroetliene ND<2.5 1.0 5.0 Vinyl Acetate "' ND<13 5.0 25 <br /> cis-1,2-Dichloroethene ND<2.5 1.0 5.0 Vinyl Chloride ° ND<2.5 1.0 5.0 <br />' <br /> trans-l,2-Dichloroethene ND<2.5 1.0 5.0 Xylenes,total 73 <br /> 1,2-Dichloropropane ND<2.5 1.0 5.0 Comments: <br /> 1,3-Dichioropropane ND<2.5 1.0 5.0 Surrogate Recoveries("/) <br /> 2,2-Dichloropropane ND<2.5 1.0 5.0 Dibromofluoromethane 106 <br />' I,1-Dichloropropene ND<2.5 1.0 5.0 Toiuene-d8 96 <br /> L0 cis-1,3-Dichloropropene ND<2.5 0 5.0 1 4-Bromofluorabenzene 97 <br /> water and vapor sampies are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> • (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy)ethene; (d) 2-hexanone; (e) dichloromethane;(f) 2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl.ester; (n) <br />' ebloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />