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I1 <br /> 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCANWBELL ANALYTICAL INC. Telephone :925-798-1620 Fax:925-798-1622 <br /> 4 http://www.mccgmpbelI.com E-mail:main@mccampbell.com <br /> Advanced GeoEnviromnental Client Project ID: Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br /> Stockton,CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client P.O: 7_Da�tealyzed: 03116-03/20/01 <br /> IVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62954 _ <br /> I Client ID MW10/03-14-01 <br /> Matrix-L W <br /> Compound Concentration" 4� ] <br /> Limit Compound Concentration` Reporting Limit <br /> S W I S <br /> Acetone(6) ND 5.0 25 trans-l,3-Dichlompropene ND 1.4 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 1-Iexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 iodometbane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> I n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND<2.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disuiflde ND 1.0 5.0 Methyl isobutyl ketone m ND 1.0 5.0 <br /> I Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chlaroethyl Vinyl Ethe ` ND 1.0 5.0 Styrene ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0F5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 <br /> 1,2-Dibronm-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.01,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.01,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.01,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 <br /> Dichlorodifluoromethane ND .1.0 5.0 1,2,3-Trichlompropane ND 1.0 5.0 <br /> 1,I-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br />' 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 1 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate ND 5.0 25 <br /> cis-1,2-Dichlormthene ND 1.0 5.0 Vinyl Chloride(d) ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br />' 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 109 <br />' 1,I-Dichloropropene ND 1.0 5.0 Toluene-l8 96 <br /> cis-l,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 99 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br />' (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) etbene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than -5 vol. 416 <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; ) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />