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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC.- Telephone : 925-7984620 Fax:925-798-1622 ' bnp://www.mccampbell_,com E-mail:main@mccampbell.cotn ' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/14/01 837 Shaw Road Date Received: 03/16/01 ' Stockton,CA 95215 Client Contact: Brian Millman Date Extracted: 03/16-03/20/01 Client P.O: Date Analyzed: 03/16-03/20/01 ' Volatile Organics By GC/MS EPA method 8260 Lab ID "62958 ' Client ID MW14/03-14-01 Matrix W Repeating Limit Repviting Limit Compound Concentration* W S Compound Concentration ' W S Acetone(b) ND<30 5.025 trans-1,3-Dichloropropene ND<5.0 1.0 5.0 Benzene 280 1.0 5.0 Ethylene dibromide ND<5.0 to 5.0 Bromobenzene ND<5.0 1.0 5A E.thyibenzene 36 1.0 5.0 ' Bromochloromethane ND<5.0 1.0 5.0 Hexachlotobutadiene ND<5.0 5.0 25 Bromodichloromethane ND<5.0 1.0 5.0 lodamethane ND<5.0 1.0 5.0 Bromoform ND<5.0 1,0 5.0 Isopropylbenzene ND<5.0 1.0 5.0 Bromomethane ND<5.0 1.0 5.0 p-Isopropyl toluene ND<5.0 1.0 5.0 n-Butyl benzene ND<5.0 1.0 5.0 Methyl butyl ketone ND<5.0 1.0 5.0 sec-Butyl benzene ND<5.0 1.0 5.0 Methylene Chloride` ND<10 1.0 5.0 tert-Butyl benzene ND<5.0 1.0 5.0 Methyl ethyl ketone Nn<5.0 2.0 10 Carbon Disulfde ND<5.0 1.0 5.0 Methyl isobutyl ketone a ND<5.0 1.0 5A '0 Carbon Tetrachloride ND<5.0 1.0 5.0 Methyl tcrt-Butyl Ether(MTBE) - 1.0 5.0 Chlorobenzene ND<5.0 1.0 5.0 Naphthalene 28 5.0 5.0 Chloroethane ND<5.0 1.0 5.0 n-Propyl benzene ND<5.0 1.0 5.0 2-Chloroethyl Vinyl Ether" ND<5.0. 19 5.0 Styrene, ND<5.0 1.0 5.0 ' Chloroform 10 1.0 5.0 1,1,1,2-Tetrachloroethane ND<5.0 1.0 5.0 Chlaromethane ND<5.0 1.0 5.0 1,1,2,2-Tetrachloroethane ND<5.0 1.0 5.0 2-Chlorotoluene ND<5.0 1.0 5.0 Tetrachloroethene ND<5.0 1.0 5.0 4-Chlorotoluene ND<5.0 1.0 5.0 Toluene 160 1.0 5.0 ' Dibromochloromethane ND<5.0 1.0 5.0 1,2,3-Trichlorobenzene ND<5.0 5.0 25 1,2-Dibromo-3-chloropropane ND<5.0 2.0 10 1,2,4-Trichlombenzene ND<5.0 5.0 25 Dibromomethane ND<5.0 1.0 5.0 1,1,1-Trichloroethane ND<5.0 1.0 5.0 1,2-Dichlorobenzene ND<5.0 1.0 5A 1,1,2-Trichloroethane ND<5.0 1.0 5.0 1,3-Dichlorobenzene ND<5.0 1.0 5.0 Trichloroethene ND<5.0 1.0 5.0 1,4-Dichlorobenzene ND<5.0 1.0 5.0 Trichlorofluoromethane ND<5.0 1.0 5.0 Dichlorodifluoromethane ND<5.0 1.0 5.0 1,2,3-Trichloropmpane ND<5.0 1.0 5.0 1,1-Dichloroethane ND<5.0 1.0 5.0 1,2,4-Trimethylbenzene 200 1.0 5.0 ' 1,2-Dichloroethane 15 1.0 5.0 1,3,5-Trimethyibenzene 82 1.0 5.0 1,1-Dichloroethene ND<5.0 1.0 5.0 Vinyl Acetate m ND<5.0 5.0 25 cis-1,2-Dichloroethene NLX5.0 I.0 5.0 Vinyl Chloride " ND<5.0 1.0 5.0 trans-1,2-Dichloroethene NLX5.0 1.0 5.0 Xylenes,total 930 ' 1,2-Dichloropropane NIX5.0 1.0 5.0 Comments: 1,3-Dichloropropane ND<5.0 1.0 FTT. Surrogate Recoveries(%} 2,2-I)ichloropropane ND<5.0 1.0 5.0Dibromotluorometha-c 109 1,1-Dichloropropene ND<5.0 1.0 5.0 Toluene-d8 97 cis-1,3-Dichloropropene ND<5.0 1.0 5.0 4-Bromofluorobenzene 98 water and vapor samples arereported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis ' (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-bexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- . pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater.than --5 vol. 9'° sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methyibenzene; (m) acetic acid ethenyl ester; (n) chloroethene;(o)dimethylbenzenes. DHS Certification No. 1644 Edward Hamilton,Lab Director