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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ® McCAWBELL ANALYTICAL INC. Telephone: 925=798-1620 Fax:925-798-1622 <br /> http://www.mccampbell.com B-mail:main@mccampbell.com <br /> • <br />' Advanced GeoEnvironmental Client Project ID:Geweke Date Sampled: 03/14/01 <br /> 837 Shaw Road Date Received: 03/16/01 <br />' Stockton,CA 95215 Client Contact:Brian Millman Date Extracted: 03/16-03/20/01 <br /> Client P.O: Date Analyzed:03/1.6-03/20/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 62957 <br />' Client ID MW13/03-14-01 <br /> Matrix W <br /> Compound Concentration* Rcporting Lunt Compound Concentration* Rcgornng Units <br />' W I S W S <br /> Acetone ca) ND 5.0 25 trans-1,3-Dichlompropcne NO 1.0 5.0 <br /> Benzene NO 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane NO 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1'0 5.0 Iodomethane NO 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene NO 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene NO 1.0 5.0 <br />' n-Butyl benzene NO 1.0 5.0 Methyl butyl ketone NO 1.0 5.0 <br /> sec-Butyl benzene NO 1.0 5.0 Methylene Chloride` NDQ.O 1.0 5.0 <br /> tort-Butyl benzene NO 1.0 5.0 Methyl ethyl ketone' ND 2.0 10 <br /> Carbon Disulfide NO 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br />' Carbon Tetrachloride ND 1.0 5.0 Methyl tent-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlorobenzene NO 1.0 5.0 Naphthalene NO 5.0 5.0 <br /> Chloroethane NO 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethe ` ND 1.0 5.0 Styrene ..ND 1.0 5.0 <br />' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane NO 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlomtoluene ND lA 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene NO lA 5.0 Toluene ND 1.0 5.0 <br />' Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene NO. 5.0 25 <br /> 1,2-Dibromo-3-chloropropane NO 2.0 l0 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane NO 1.0 5.0 1,1,1-Trichloroethane NO 1.0 5.0 <br /> 1,2-Dichlorobenzene NO 1.0 5.0 1,1,2-Trichloroethane NO 1.0 5.0 <br />' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5"0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichlompropane ND 1.0 5"0 <br /> 1,1-Dichloroethane NO 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br />' 1,2-Dicbloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Diehloroethene ND 1.0 5.0 Vinyl Acetate"I ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br />' trans-1,2-Dichloroethene NO 1"0 5.0 Xylenes,total NO 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane NO - 1.0 5.0 Dibromofluoromethane 111 <br />' <br /> 1,1-Dichloropropene NO 1.0 3 Toluene-d8 96 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobertzene 98 <br /> 'water and vapor samples are reported in ug(L,soil and sludge samples in ug/kg,wipes in uVwipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means analyte nat applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than-5 vol, % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1 methylbenzene; (m) acetic acid ethenyl"ester; (n) <br />' chioroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Harrl,ilton,Lab Director <br /> 1 <br />