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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax . 925-798-1622 <br /> http://www,mccampbell.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received. 01/19/00 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 01/21-01/24/00 <br /> Client P.O: Date Analyzed: 01/21-01/24/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 29320 <br /> Client ID MW-1211-18-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone(b) ND<30 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromoeblorometbane ND Hexachlorobutadiene ND <br /> BrumodichlOTOmethane ND lodomethane ND <br /> Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone'E' ND <br /> sec-Butyl benzene ND Methylene Chloride" ND<10 <br /> tert-Butyl benzene ND Methyl ethyl ketone" ND <br /> Carbon Disulfide ND Methyl isobutyl ketone'6' ND <br /> Carbon Tetrachloride ND Methyl tent-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether"' ND Styrene` ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene"IND <br /> Dibromochloromethane ND 1,2,3-Trichiorobenzene ND <br /> 1,2-Dib7-omo-3-chl0r0pr0pane ND 1,2,4-Trichlorobenzene ND <br /> Dlbromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND "I'richlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ND <br /> Iran s-1,2-Dichloroethen e ND Xylenes,total ` ND <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries('Yo) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 110 <br /> ],1-Dichloropropene ND Toluene-dS 103 <br /> cis-1,3-Dichloropropene ND H 4-Bromofluorobenzene 96 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug1L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy)ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-bwanone; (g)4-methyl-2- <br /> pentanone or isopropyl acetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than—5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />