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110 2nd Avenue South,,#D7,Pacheco,CA 9,4553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> httpa/www.mccam�bell.com £-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 01121-01124100 <br /> Client P.O: Date Analyzed: 01121-01/24100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 29321 <br /> Client 1D MW-1411-18-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<30 trans-1,3-Dichloropropene ND<2.5 <br /> Benzene 63 Ethylene dibromide ND<2.5 <br /> Bromobenzene ND<2.5 Ethylbenzene 29 <br /> Bromochloromethane ND<2.5 Hexachlorobutadiene 8.2 <br /> Bromodichloromethane ND<2.5 lodomethane ND<2.5 <br /> Bromoform ND<2.5 lsopropylbenzene 6.6 <br /> Bromomethane ND<2.5 p-Isopropyl toluene ND<2.5 <br /> n-Butyl benzene 3.8 Methyl butt'!ketone' ND<2.5 <br /> sec-Butyl benzene ND<2.5 Methylene Chloride" ND<10 <br /> ten-Butyl benzene 9.0 Methyl ethyl ketone"' ND<2.5 <br /> Carbon Disulfide ND<2.5 Methyl isobutyl ketone'g ND<2.5 <br /> Carbon Tetrachloride ND<2.5 Methyl tent-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<2.5 Naphthalene 18 <br /> Chloroethane ND<2.5 n-Propyl benzene 7.8 <br /> 2-Chloroethyl Vinyl Ether"' ND<2.5 Styrene` ND<2.5 <br /> Chloroform ND<2.5 1,1,1,2-Tetrachloroethane ND<2.5 <br /> Chloromethane ND<2.5 1,1,2,2-Tetrachloroethane ND<2.5 <br /> 2-Chlorotoluene ND<2.5 Tetrachloroethene ND<2.5 <br /> 4-Chlorotoluene ND<2.5 Toluene "' 30 <br /> Dibromochloromethane ND<2.5 1,2,3-Trichlorobenzene 29 <br /> 1,2-Dibromo-3-chloropropane ND<2.5 1.2,4-Trichlorobenzene 5.7 <br /> Dibromomethane ND<2.5 1,1,1-Trichloroethane ND<2.5 <br /> 1,2-Dichlorobenzene ND<2.5 1,1,2-Trichloroethane ND<2.5 <br /> 1,3-Dichloroben2ene ND<2.5 Trichloroethene ND<2.5 <br /> 1,4-Dichlorobenzene ND<2.5 Trichlorofluoromethane ND<2.5 <br /> Dichlorodifluoromethane ND<2.5 1.2,3-Trichl oropropane ND<2.5 <br /> 1,1-Dichloroethane ND<2.5 1,2,4-Tri methylbenzene 90 <br /> 1,2-Dichloroethane 12 1,3,5-Trimethylbenzene 24 <br /> 1,1-Dichloroethane ND<2.5 Vinyl Acetate"' 7.3 <br /> cis-1,2-Dichloroethene ND<2.5 Vinyl Chloride I ) ND<2.5 <br /> trans-1,2-Dichloroethene ND<2.5 Xylenes,total W190 <br /> 1,2-Diehl oropropane ND<2.5 Comments: <br /> 1,3-Dichloropropane ND<2.5 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<2.5 Dibromofluaromethane 128 <br /> LI-Dichloropropene ND<2.5 Toluene-d8 109 <br /> cis-1,3-Dichloropropene ND<2.5 4-BromoflUOiobenzene 87 <br /> '%nater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipc and al]TCLP/SPLP extracts in uglL <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-prop2none or dimethyl ketone; (c)(2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-bumnone; (g) 4-methyl-2- <br /> pentanone or isopropyl acetone; (h)lighter than water immiscible sheen is present;(i) liquid sample that contains greater than -5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />