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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> httR://www.mccamt)bell-com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/l 8/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 01/21-01/24/00 <br /> Client P.O: Date Analyzed: 01/21-01/24/00 <br /> EPA method 8260 modified Oxygenated Volatile Organics By GC/MS <br /> Lab ID 29319 29320 29321 <br /> MW-11/1- MW-12/I- MW-14/1- Reporting Limit <br /> Client ID 18-00 18-00 18-00 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND<2.5 5.0 1.0 <br /> Ethyl ten-Butyl Ether(ETBE) ND ND ND4.5 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND PND12.5 <br /> 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND 5.0 1.0 <br /> ten-Butanol ND ND ND<13 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromolluoromethane 104 110 128 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol. %sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No.'1644 Edward Hamilton, Lab Director <br />