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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax : 925-798-1622 <br /> ht-tp://www.mccamt)bell.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 01/18/00 <br /> 4005 North Wilson Way Date Received: 01/19/00 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 01/21-01/24/00 <br /> Client P.O: Date Analyzed: 01/21-01/24/00 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 29315 29316 29317 29318 <br /> MW-6/1-18- MW-7/1-18- MW-811-18- MW-911-18- Reporting Limit <br /> Client ID 00 00 00 00 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND<2.5 ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND<2.5 ND. 5.0 Lo <br /> Methyl-tert Buty]Ether(MTBE) ND ND ND<2.5 ND 5.0 1.0 <br /> tert-Amy!Methyl Ether(TAME) ND ND ND<2.5 ND 5.0 1.0 <br /> tert-Butanol ND ND 27 16 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 114 300 99 99 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />• <br />