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' 110n <br /> 2 d Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax:925-798-1622 <br />' hh:Uwww.mccampbeil.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 09/30/99 <br /> 4005 North Wilson Way Date Received: 10/02/99 <br />' Stockton, CA 95205 Client Contact:Kevin McKibben Date Extracted: 10/07-10/12/99 <br /> Client P.O: Date Analyzed: 10/07-10/12/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 22679 <br />' Client ID MW8 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone' I ND<60 trans-l,3-Dichloropropene ND<10 <br /> Benzene ND<10 Ethylene dibromide ND<10 <br /> Bromobenzene ND<10 Ethylbenzene 170 <br /> Bromochloromethane ND<l0 Hexachiorobutadiene ND<l0 <br />' Bromodichloromethane ND<10 lodomethane ND<10 <br /> Bromoform ND<10 Isopropylbenzene 73 <br /> Bromomethane ND<10 p-Isopropyl toluene ND<10 <br /> n-Butyl benzene ND<10 Methyl butyl ketone ND<10 <br />' sec-Butyl benzene 20 Methylene Chloride" ND<40 <br /> tent-Butyl benzene ND<10 Methyl ethyl ketone N1><10 <br /> Carbon Disulfide NIK10 Methyl isobutyl keton7e ND<10 <br /> Carbon Tetrachloride ND<10 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<10 Naphthalene ND<10 <br /> Chloroethane ND<10 n-Propyl benzene 110 <br /> 2-Chloroethyl Vinyl Ether" ND<10 Styrene` ND<10 <br /> Chloroform NLK 10 1,1,1,2-Tetrachloroethane ND<10 <br /> Chlorometban a ND<10 1,1,2,2-Tetrachloroethane ND<10 <br /> 2-Chlorotoluene ND<10 Tetrachloroethene ND<10 <br /> 4-Chlorotoluene ND<10 Toluene"' ND<10 <br /> Dibromochloromethane ND<10 1,2,3-Trichlorobenzene ND<10 <br />' <101,2-Dibromo-3-chloropropane ND<10 1,2,4-Trichlorobenzene ND<10 <br /> Dibromomethane ND<10 1,1,1-Trichloroethane ND<l 0 <br /> 1,2-Dichlorobenzene ND<10 1,1,2-Trichloroethane ND<10 <br /> 1,3-Dichlorobenzene ND<10 Trichloroethene ND<10 <br /> I 1,4-Dichlorobenzene ND<]0 Trichlorofluoromethane ND<10 <br /> Dichlorodifluoromethane ND<10 1,2,3-Trichloropropane ND<10 <br /> l,]-Dichloroethane ND<10 1,2,4-Trimethylbenzene 330 <br /> 1,2-Dichloroethane 24 1,3,5-Trimethylbenzene 61 <br /> 1,1-Dichloroethene ND<10 Vinyl Acetate " ND<10 <br /> cis-1,2-Dichloroethene ND<10 Vinyl Chloride'° ND<]0 <br /> trans-l,2-Dichloroethene ND<10 Xylenes,total ° 190 <br />�- 1,2-Dichloroprop2ne ND<10 Comments: <br /> 1,3-Dichloropropane ND<10 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<10 Dibromofluoromethane 105 <br /> 1,1-Dichloropropene ND<]0 Toluene-d8 100_ <br /> cis-1,3-Dichloropropene ND<10 4-Bromofluorobenzene 95 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br />' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane-, (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than •-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />