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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> A <br /> MICAPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mccampbell.cotn <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 09/30/99 <br /> 4005 North Wilson Way Date Received: 10/02/99 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted 10/07-10112199 <br /> Client P.O: Date Analyzed: 10107-10112/99 <br /> I Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 22673 22674 22675 22676 <br /> Reporting Limit <br /> Client ID MW6 MWI2 MW11 MW9 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(RIPE) ND ND ND ND<10 5 0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND<10 5.0 1.0 <br /> • Methyl-tert Butyl Ether(MTBE) ND ND ND ND<10 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND<10 5.0 1.0 <br /> tert-Butanol ND 7.6 ND 48 25 5.0 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 120 120 120 99 <br /> Comments: <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> I (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 `Edward Hamilton, Lab Director <br /> r <br /> I <br />