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4 <br /> 110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> [�::7WCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> s, http/lwww mccampbell com E mail main®mccampbell corn <br /> Advanced GcoEnvnronmental,Inc Client Project ID Cherokee Trucking Date Sampled 08/29/02 <br /> 837 Shaw Road Date Received 08/30/02 <br /> Client Contact Paul Dotson Date Extracted 08130/02-09/06/02 <br /> Stockton, CA 95215 <br /> Client P O [Late Analyzed 08130102-09106102 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS (Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0208519 <br /> Lab ID 0208519-004C <br /> Client 1D UST5/082902 <br /> Matrix Water <br /> Compound Concentration * DF Limits Compound Concentration * DF �; 2g <br /> Acetone ND<50 10 50 tert-Amyl methyl ether(TAME) ND<5 0 10 05 <br /> Benzene ND<5 0 10 0 5 Bromobenzene ND<5 0 10 0 5 <br /> Bromochloromethane ND<5 0 10 0 5 Bromodichloromethane ND<5 0 10 0 5 <br /> Bromofonn ND<5 0 10 0 5 Bromomethane ND<5 0 10 0 5 <br /> 2-Butanone(MEK) ND<10 10 1 0 t-Butyl alcohol(TBA) NDe50 10 5 0 <br /> n-Butyl benzene ND<5 0 10 0 5 sec-Butyl benzene ND<5 0 10 0 5 <br /> tert-Butyl benzene ND<5 0 10 0 5 Carbon Disulfide ND<5 0 10 0 5 <br /> Carbon Tetrachloride ND<5 0 10 0 5 Chlorobenzene ND<5 0 10 0 5 <br /> Chloroethane ND<5 0 10 0 5 2-Chloroethyl Vinyl Ether ND<10 10 10 <br /> Chloroform ND<5 0 10 0 5 Chloromethane ND<5 0 10 05 <br /> 2-Chlorotoluene ND<5 0 10 05 4-Chlorotoluene ND<5 0 10 0 5 <br /> Dibromochloromethane ND<5 0 10 0 5 1,2-Dibromo-3-chloropropane ND<10 10 1 0 <br /> 1,2-Dibromoethane(EDB) ND<5 0 10 0 5 Dibromomethane ND<5 0 10 0 5 <br /> 1,2-Dichlorobenzene ND<5 0 10 0 5 1,3-Dichlorobenzene ND<5 0 10 0 5 <br /> 1,4-Dichlorobenzene ND<5 0 10 05 Dichlorodifluoromethane ND<5 0 10 0 5 <br /> • 1,I-Dichloroethane N13<5 0 10 05 1,2-Dichloroethane(1,2-DCA) 440 10 05 <br /> 1,1-Dichloroethene ND<5 0 10 05 cis-1,2-Dichloroethene ND<5 0 10 0 5 <br /> trans-1,2-Dichloroethene ND<5 0 10 0 5 1,2-Dichloropropane ND<5 0 10 0:5 <br /> 1,3-Dichlorapropane ND<5 0 10 05 2,2-Dichloropropane ND<5 0 10 05 <br /> 1,1-Dichloropropene ND<5 0 10 05 cis-1,3-Dichloropropene ND<5 0 10 0 5 <br /> trans-1,3-Dichloropropene ND<5 0 10 0 5 Dnsopropyl ether(DIPS) NDc5 0 10 05 <br /> Ethylbenzene ND<5 0 10 0 5 Ethyl tert-butyl ether(ETRE) ND<5 0 10 05 <br /> Hexachlorobutadiene ND<50 10 5 0 2-Hexanone ND<5 0 10 0 5 <br /> Iodomethane(Methyl iodide) ND<5 0 i0 0 5 Isopropylbenzene ND<5 0 10 0 5 <br /> 4-Isopropyl toluene ND<5 0 10 0 5 Methyl-t-butyl ether(MTBE) ND<5 0 10 0 5 <br /> Methylene chloride ND<5 0 10 0 5 4-Methyl-2-pentanone(MIBK) ND<5 0 10 0 5 <br /> Naphthalene ND<50 10 5 0 n-Propyl benzene ND<5 0 10 0 5 <br /> Styrene ND<5 0 10 0 5 1,1,1,2-Tetrachloroethane ND<5 0 10 0 5 <br /> 1,1,2,2-Tetrachloroethane ND<5 0 10 0 5 Tetrachloroethene ND<5 0 10 0 5 <br /> Toluene ND<5 0 10 0 5 1,2,3-Tnchlorobenzene ND<5 0 10 0 5 <br /> 1,2,4-Tnehlorobenzene ND<5 0 10 0 5 1,1,1-Trichloroethane ND<5 0 10 0 5 <br /> 1,1,2-Tnchloroethane ND<5 0 10 0 5 Tnchloroethene ND<5 0 10 0 5 <br /> Tnehlorofluoromethane ND<5 0 10 0 5 1,2,3-Tnchloropropane ND<5 0 10 0 5 <br /> 1,2,4-Tnmethylbenzene ND<5 0 10 0 5 1,3,5-Tnmethylbenzene ND<5 0 10 0 5 <br /> Vinyl Acetate ND<50 10 5 0 Vinyl Chloride ND<5 0 10 0 5 <br /> Xylenes ND<5 0 10 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 114 %SS2 106 <br /> %SS3 t 929 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sbcen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />