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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCaanpbell Analytical Inc <br /> Tel <br /> 925 798-1620 Fax 925-798-1622 <br /> http//www mecampbell com E mail main@mecampbell corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Cherokee Trucking Date Sampled 08/29/02 <br /> 837 Shaw Road Date Received 08/30/02 <br /> Client Contact Paul Dotson Date Extracted 08/30/02-09/06102 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 08/30102-09106102 <br /> Volattles Organics+Oxygenates by P&T and GC/MS (Basic Target List)* <br /> Extmcunn Method SW5030B Analytical Method SW8260B Work Order 0208519 <br /> Lab ID 0208519-005C <br /> Client ID UST61082902 <br /> Matrix Water <br /> Compound Concentration* DF `Ys Compound Concentration * DF ,N <br /> Acetone ND 10 1 .50 tert-Amyl methyl ether(TAME) ND 1 0 05 <br /> Benzene ND 10 05 Bromobenzene ND 10 05 <br /> Bromochloromethane ND 10 05 Bromodichlorvmethane ND t 0 05 <br /> Bromoform NO 10 05 Bromomethane ND 1 0 05 <br /> 2-Butanone(MEK) ND 10 10 t-Butyl alcohol(TBA) ND 10 50 <br /> n-Butyl benzene ND 10 05 sec-Butyl benzene ND 10 05 <br /> tert-Butyl benzene ND 1 0 05 Carbon Disulfide ND 10 05 <br /> Carbon Tetrachloride ND 1 0 05 Chlorobenzene ND 10 05 <br /> Chloroethane ND 1 0 05 2-Chloroethyl Vinyl Ether ND 10 10 <br /> Chloroform ND 1 0 05 Chloromethane ND 10 05 <br /> 2-Chlorotoluene ND 1 0 05 4-Chlorotoluene ND 1 0 05 <br /> Dibromochloromethane ND 1 0 05 1,2-Dibromo-3-chloropropane ND 10 10 <br /> 1,2-Dihromoethane(EDB) ND 10 05 Dibromomethane ND 10 05 <br /> 1,2-Dichlorobenzene ND 10 05 1,3-Dichlorobenzene ND 10 05 <br /> 1,4-Dichlorobenzene ND 10 05 Dichlorodifluoromethane ND 10 05 <br /> I,1-Dichloroethane ND 10 05 1,2-Dichloroethanc(1,2-DCA) 44 10 05 <br /> 1,1-Dichloroethene ND 10 05 cis-1,2-Dichloroethene ND 10 05 <br /> trans-1,2-Dichloroethene ND 10 05 1,2-Dichloropropane ND to 05 <br /> 1,3-Dichloropropane ND 10 05 2,2-Diebloropropane ND 10 05 <br /> 1,1-Dichloropropene ND 10 05 cis-1,3-Dichloropropene ND 10 05 <br /> trans-1,3-Dichloropropene ND 10 05 Di sopropyl ether(DIPS) ND 1 10 05 <br /> Ethylberizene ND 1 0 05 Ethyl tert-butyl ether(ETBE) ND 1 0 05 <br /> Hexachlorobutadiene ND 1 0 50 2-Hexanone ND 10 05 <br /> Iodomethane(Methyl Iodide) ND 1 0 05 Isopropylbenzene ND 1 0 05 <br /> 4-Isopropyl toluene ND 10 05 Methyl-t-butyl ether(MTBE) 072 1 0 05 <br /> Methylene chloride ND 10 05 4-Methyl-2-pentanone(MIBK) ND 10 05 <br /> Naphthalene ND 10 50 n-Propyl benzene ND 10 05 <br /> Styrene ND 10 05 1,1,1,2-Tetrachloroethane ND 10 05 <br /> 1,1,2,2-Tetrachloroethane ND 10 05 Tetrachloroethene ND 1 0 05 <br /> Toluene ND 10 05 1,2,3-Tnehlorobenzene ND 10 05 <br /> 1,2,4-Tnchlorobenzene ND 10 05 1,1,1-Trichloroethane ND 10 05 <br /> 1,1,2-Tnehloroethane ND 1 0 05 Trichloroethene ND 10 05 <br /> Trichlorofluoromethane ND 10 05 1,2,3-Tnehloropropane ND 1 ❑ 0 5 <br /> 1,2,4-Tnmethylbenzene ND 10 05 1,3,5-Tnmethylbenzene ND 1 0 0 5 <br /> Vinyl Acetate ND 10 50 Vinyl Chloride ND 1 0 0 5 <br /> X lenes ND to 05 <br /> Surrogate Recoveries(%) <br /> %SSI 114 %SS2 923 <br /> %SS3 986 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludgelsolid samples in ug/kg, wipe samples in ug/wtpe, <br /> productloil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,1)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />