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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> }lMi_1Lwww mccgmpbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cherokee Trucking Date Sampled 06/14/00 <br /> 4005 North Wilson Way Date Received 06/15/00 <br /> Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 06/16-06119/00 <br /> Client P O Date Analyzed 06/16-06/19/00 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br />' Lab ID 40407 <br /> Client ID DW-1106-14-00 <br /> Matrix W <br /> Repwbng Limit Rcportmg Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone(b) ND 50 25 trans-1,3-Dichloivpropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 10 50 liexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 10 5 0 p4sopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride` ND to 50 <br /> cert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND 1 0r5no <br /> Carbon Tetrachloride ND 1 0 50 Methy{Cert-Butyl Ether(MTBE) --- 1 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 1 0 <br />' 2-Chloroethyl Vinyl Ether` ND 1 0 50 Styrene ND 10 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND - 1 0 5 0 <br /> 2-Chlorotoluene - ND 10 50 Tetrachloroethene K , 64 10 1 50 <br />' 4-Chlorotoluene ND 10 50 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibmmo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 10 50 Tnchlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND 1 0 50 <br /> 1,1-Dichloroethane 1 3 1 0 50 1,2,4-Trimethyl6enzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Trnnethylbenzenc ND 1 0 50 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride ¢ ND 10 50 <br /> I trans-l,2-Dichlomethene ND 10 5 0 Xylenes,total ND 1 0 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dbromofluoromethane 128 <br /> 1,1-Dichloropropene ND 10 5 0 Toluene-d8 130 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 97 <br /> "water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2- <br /> pentarione or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol °/a <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 r7.V Edward Hamilton,Lab Director <br />