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g, 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> ® McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br />' http//www mccampbell coin E-mail main@mccarripbell corn
<br /> Advanced GeoEnvironmental Client Protect M Cherokee Trucking Date Sarrtpted 06/14/00
<br /> 4005 North Wilson Way Date Received 06/15/00
<br />' Stockton, CA 95205 Client Contact Tony Mikacich Date Extracted 06/16-06/19/00
<br /> Client P O Date Analyzed 06/16-06/19/00
<br />' Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 40408
<br />' Client ID DW-2/06-14-00
<br /> Matrix W
<br /> Reporting Lnntt * Reporting Limit
<br /> Compound Concentration* W S Compound Concentration W S
<br />' Acetone m> ND 50 25 trans-l,3-Dtchloropropene ND 10 50
<br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 5 0
<br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 5 0
<br />' Bromochloromethane ND 10 5 0 Hcxachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 50
<br /> Bromoform ND 10 5 0 [sopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 50
<br />' n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 5 0
<br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND 10 50
<br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND 1 0 5 0
<br /> Carbon Tetrachloride ND 10 50 Methyl tent-Butyl Ether(MTBE) — 10 50
<br /> Chlorebenzene ND 10 50 Naphthalene ND 50 50
<br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 50
<br /> 2-Chloroethyl Vinyl Ether"' ND 10 5 0 Styrene ND to 50
<br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND - 10 50
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND<2 0 10 5 0
<br /> 1 4-Chlorotoluene ND 1 0 50 Toluene ND 10 5 0
<br /> Dibromochloromethane ND 10 5 0 1,2,3-Trtchlorobcnzene ND 5 0 25
<br /> 1,2-Dibmmo-3-chloropropane ND 2 0 10 1,2,4-Trtchlorobenzene ND 5 0 25
<br /> Dibromomethane ND rio
<br /> 50 1,1,1-Tnchloroethane ND 10 50
<br />' 1,2-Dichlorobenzene ND 5 0 1,1,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 50 Tnchloroethena ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 5 0 Trichlorofluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND 5 0 1,2,3-Tnchloropropane ND 10 5 0
<br />' 1,1-Dichloroethane ND 50 1,2,4-Trimethylbenzene ND 10 50
<br /> 1,2-Dicbloroethane ND 50 1,3,5-Trimethylbenzene ND to 50
<br /> l,l-Dichloroethene ND 1 0 50 Vinyl Acetate tJ ND 50 i 25
<br /> cis-1,2-Dichloroethene ND to 5 0 Vinyl Chloride " ND 10 5 0
<br />' trans-1,2-Dichloroethene ND 10 5 0 Xylenes,total ND 1 0 50
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane 124
<br />' 1,1-Dichloropropene ND to 50 TolueneA8 110
<br /> cis-1,3-Dtchloropropene ND l 0 5 0 4-Bromofluorobenzene � 94
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanonc or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hanulton,Lab Director
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