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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC //wTelephone 925-798-1620 Fax 925-798-1622 <br /> hup ww mccamabell co m E-mail mam@?a mecampbell com <br /> iAdvanced GeoEnvtronmental Client Protect ID Cherokee Truck Stop Date Sampled 03/20/00 <br /> 4005 North Wilson Way Date Received 03/23/00 <br /> iStockton, CA 95205 Client Contact Kevin McKibben Date Extracted 03/25-03/28/00 <br /> Client P O Date Analyzed 03/25-03/28/00 <br /> iVolatile Organics By GC/MS <br /> EPA method 8260 <br /> i Lab ID 33735 <br /> Client ID UST3/3-20-00 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone NDc2 0 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> i Bromodichloromethane ND lodomethane ND <br /> BTomoforrri ND Isopropylbenzene ND <br /> Bromomethane ND p-isopropyl toluene ND <br /> n-Butyl benzene ND Methyl bury]ketone ND <br /> i sec-Butyl benzene ND Methylene Chlonde` ND<2 0 <br /> ten-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone 18 ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether" ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene") ND <br />' Dibminochloromethanc ND 1,2,3-Trichiorobenzene ND <br /> 1 2-Dibromo 3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnchioroethane ND <br />' 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Tnehlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1 2 3-Tnehloroprop2ne ND <br /> IJ-Dichloroethane ND 1,2,4-Tnmethylbenzene ND <br />' 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzene ND <br /> I 1-Dichloroethene ND Vinyl Acetate "' ND <br /> cis-1,2-Dichloroethene ND Vinyl Chlonde 01 ND <br /> trains-l,2-Dichloroethene ND Xylenes,total ND <br />' 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate RecoNtries{°/a) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 102 <br /> l,]-Dichloropropene ND Toluene-d8 101 <br />' cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 107 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in uglwipe and all TCLP/SPLP extracts in ug/L <br /> Reporting hmits unless otherwise stated water samples I ug/L %apor samples 0 5 ug/L solid and sludge samples 5 ug/kg wipes 0 Zug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy)ethene, (d) 2-hexanone, (e)dichloromethane, (f) 2-butanone, (g)4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acrd ethenyl ester, (n) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />